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Preparation method for water soluble compound cooling agent

A cooling agent, water-soluble technology, applied in the field of preparation of water-soluble compound cooling agent, can solve the problem of cooling agent insoluble in water, etc., and achieve the effect of broadening the application range

Inactive Publication Date: 2015-12-23
ANHUI AIDI SPICE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The compounded cooling agent has soft, long-lasting, and no bitter taste. At the same time, the invention also solves the problem that the cooling agent is insoluble in water, and can be widely used in food, daily chemical, beverage and other products

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] This embodiment relates to a preparation method of a water-soluble compound cooling agent, comprising the following steps:

[0023] Step (1): Mix Tween-80 and poloxamer evenly at a mass ratio of 2:1 to obtain solution A;

[0024] Step (2): Mix 2,6-dimethyl-β-cyclodextrin and hydroxypropyl-β-cyclodextrin at a mass ratio of 1:1, add to the solution A, and vibrate with an ultrasonic oscillator After treatment for 0.5h, the ultrasonic frequency was controlled at 25KHZ to obtain solution B;

[0025] Step (3): Mix L-menthol, cooling agent WS-23, and WS-5 at a mass ratio of 3:1:1, add to dipropylene glycol solution for dissolution, and compound cooling agent and dipropylene glycol The mass ratio of propylene glycol is 1:3. After it is completely dissolved, it is added to solution B, stirred and mixed evenly, and the product is obtained.

Embodiment 2

[0027] This embodiment relates to a preparation method of a water-soluble compound cooling agent, comprising the following steps:

[0028] Step (1): Mix Tween-80 and poloxamer evenly at a mass ratio of 5:1 to obtain solution A;

[0029] Step (2): Mix 2,6-dimethyl-β-cyclodextrin and hydroxypropyl-β-cyclodextrin at a mass ratio of 3:1, add to the solution A, and vibrate with an ultrasonic oscillator After treatment for 3 hours, the ultrasonic frequency was controlled at 40KHZ to obtain solution B;

[0030] Step (3): Mix L-menthol, cooling agent WS-23, and WS-5 at a mass ratio of 5:3:3, add to dipropylene glycol solution for dissolution, and compound cooling agent and dipropylene glycol The mass ratio of propylene glycol is 1:10. After it is completely dissolved, it is added to solution B, stirred and mixed evenly, and the product is obtained.

Embodiment 3

[0032] This embodiment relates to a preparation method of a water-soluble compound cooling agent, comprising the following steps:

[0033] Step (1), mix Tween-80 and poloxamer uniformly according to the mass ratio of 3:1 to obtain solution A;

[0034] Step (2), mix 2,6-dimethyl-β-cyclodextrin and hydroxypropyl-β-cyclodextrin at a mass ratio of 2:1, add to the solution A, and vibrate with an ultrasonic oscillator After treatment for 1.5h, the ultrasonic frequency was controlled at 35KHZ to obtain solution B;

[0035] Step (3), mix L-menthol, cooling agent WS-23, WS-5 at a mass ratio of 5:3:1, add to dipropylene glycol solution for dissolution, and compound cooling agent and dipropylene glycol The mass ratio of propylene glycol is 1:5. After it is completely dissolved, it is added into solution B, stirred and mixed evenly, and the product is obtained.

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Abstract

The present invention relates to a preparation method for a water soluble compound cooling agent. The preparation method comprises the following steps: step (1) uniformly mixing Tween-80 and poloxamer to obtain solution A; (2) adding poloxamer into the solution A and oscillating the solution A with ultrasound wave to obtain solution B; step (3) dissolving a compound cooling agent in dipropylene glycol, adding the obtained solution into solution B, and uniformly mixing the solution by stirring to obtain the water soluble compound cooling agent. According to the present invention, a plurality of cooling agents are compounded according to a certain ratio, the compounded cooling agent has a gentle and lasting cooling flavor, and has no bitterness. Meanwhile, the problem that the cooling agent is insoluble in water is solved, and the water soluble compound cooling agent can be widely used in foods, daily products, beverages and other products.

Description

technical field [0001] The invention belongs to the application field of cooling agents, and in particular relates to a preparation method of a water-soluble compound cooling agent. Background technique [0002] Cooling agent is a general term for all chemical substances that can produce a cooling effect and are not strong in medicinal properties. Levomenthol is the most traditional cooling agent. Because it can give products a cool and fresh feeling, it has been widely used in food, medicine, daily chemicals, tobacco and other industries. But its shortcomings are also very obvious: bitter taste and pungent smell, cooling effect is not obvious when the dosage is low, strong volatility and short-term effect, almost insoluble in water and strong irritation to eyes, etc. Due to the above-mentioned disadvantages of levomenthol, its use in many products is limited. In order to overcome the above-mentioned shortcomings of the traditional cooling agent L-menthol, new cooling agen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/226A23L2/52
CPCA23L2/52
Inventor 刘锐锋郑俊峰文汉张雪梅李敏何光良
Owner ANHUI AIDI SPICE CO LTD
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