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A kind of nickel-carbon-iron-based powder metallurgy alloy and preparation method thereof

An iron-based powder metallurgy and nickel-carbon technology, which is applied to powder metallurgy low-alloy steel with carbon elements and its preparation, increases the field of nickel, and can solve the problem that the plasticity of iron-based powder metallurgy materials has not been significantly improved and the factors affecting plasticity have not Relatively sufficient explanation and research, alloy plasticity has not been significantly improved, etc., to achieve the effect of good plasticity and microstructure that is conducive to popularization and application

Inactive Publication Date: 2017-04-26
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Subsequently, the alloy prepared by adding C element in Fe-Ni not only reduces the cost of powder metallurgy products, but also obtains better performance. After quenching, its tensile performance can exceed 800MPa, but the alloy after quenching Plasticity has not been significantly improved
[0008] Fe-Ni-C powder metallurgy has been widely used because of its good mechanical properties, but the influence of Ni and C in Fe-Ni-C powder metallurgy materials on the properties of iron-based powder metallurgy products and the microstructure There are few studies on the changes of iron-based powder metallurgy materials. A lot of research has been done on the mechanical properties of iron-based powder metallurgy at home and abroad, and the strength and hardness of the alloy have been greatly improved, but the plasticity of iron-based powder metallurgy materials has not been obtained. It is obviously improved, and at the same time, the factors affecting the plasticity of iron-based powder metallurgy materials by adding elements have not been fully explained and studied, and its application range is still limited so far.

Method used

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  • A kind of nickel-carbon-iron-based powder metallurgy alloy and preparation method thereof
  • A kind of nickel-carbon-iron-based powder metallurgy alloy and preparation method thereof
  • A kind of nickel-carbon-iron-based powder metallurgy alloy and preparation method thereof

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Experimental program
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Embodiment 1

[0032] (1) LAP100.29 water atomized iron powder is used as raw material, colloidal graphite and carbonyl nickel powder are used as raw materials for adding carbon and nickel alloying elements respectively, and nickel-carbon-iron-based materials are prepared according to the ratio in Table 1 (the balance is Iron), add zinc stearate (ZnSt 2 ) as a release agent.

[0033] (2) Ball milling and mixing: during mixing, 500g of the material in step (1) is used as a mixing batch, and the powder is milled using a horizontal ball mill. The material of the ball milling tank is stainless steel, and the steel ball material is stainless steel. The ball-to-material ratio is 2: 1. The rotating speed of the spherical tank is set to 200r / min, the ball milling time is 8 hours, and the protective atmosphere is not used.

[0034] (3) Put the material in step (2) into the mold and press to form.

[0035] (4) Bury the material in step (3) in the refractory sand in the sintering furnace, the sinteri...

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Abstract

The invention discloses a nickel-carbon-iron-based powder metallurgy alloy and a preparation method thereof. The alloy includes raw materials in the following weight percentages: Ni-(1-7)wt%, C-(0.4-1)wt%, Fe-(92-94.6)wt%. The production process includes the following steps: (1) Ball milling and mixing: the nickel, the carbon and the iron materials are mixed by ball milling, the ball-to-material ratio is (1-3):1, and the rotating speed of the spherical tank is set to 200-400r / min. The ball milling time is 6-8 hours; (2) the material mixed by ball milling in step (1) is loaded into a mold, and pressed into a mold; (3) the material pressed and formed in step (2) is buried in refractory sand and heated at 1100 ° C After sintering at ‑1200°C for 1‑2h, the nickel-carbon-iron-based powder metallurgy alloy is obtained by cooling in the furnace. The protective atmosphere during the sintering process is (90‑100)%N2+(0‑10)%H2. In the present invention, nickel and carbon elements are added in iron-based powder metallurgy, and a suitable ball milling process is selected, so that the manufactured alloy has a better microstructure, smaller porosity, spheroidized pores, and smaller grain size, thereby obtaining a hardness Iron-based powder metallurgy material with high tensile strength and good plasticity.

Description

technical field [0001] The invention relates to the field of iron-based powder metallurgy, in particular to a powder metallurgy low-alloy steel with nickel and carbon added and a preparation method thereof. Background technique [0002] Powder metallurgy technology has many unique advantages in material research and development and material processing, the most important of which are as follows: [0003] (1) Alloy materials prepared by powder metallurgy technology have very unique chemical and physical properties compared with materials prepared by traditional processes. Materials that cannot be prepared by traditional casting methods and mechanical methods, as well as many processed parts of refractory metals (such as hard alloys, functional ceramics, etc.) can be realized by powder metallurgy technology. [0004] (2) In the process of powder metallurgy material preparation, the composition and the addition amount of elements in the alloy can be easily changed. The element...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C38/08C22C33/02
Inventor 宫建红张修齐曹昀刘盛男杨丽民
Owner SHANDONG UNIV
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