A kind of catalyst for high activity fluid bed
An activator and catalyst technology, applied in the field of high-activity fluid bed catalysts, can solve the problems of poor catalyst efficiency and reduced catalytic capacity, and achieve the effect of ensuring effective use, high activity and improving use efficiency
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Embodiment 1
[0024] A catalyst for a high-activity fluid bed, which includes a three-layer activator and a carrier; the carrier is a zeolite molecular sieve, the first layer of catalyst is an active metal oxide catalyst, and the second layer of catalyst is platinum-doped oxidation Aluminum nano catalyst, the third layer of catalyst is molybdenum oxide catalyst.
[0025] The catalyst is divided into three parts, the first part is the active metal oxide catalyst, the second part is the lining active metal oxide catalyst, the outer surface is covered with a platinum-doped alumina nano-catalyst, and the third part is the lining Active metal oxide catalyst, the middle layer is coated with platinum-doped alumina nano-catalyst, and the outer layer is molybdenum oxide catalyst.
[0026] The ratio of the active metal oxide catalyst, the platinum-doped alumina nano-catalyst and the molybdenum oxide catalyst is 4:2:1.
[0027] The metal oxide catalyst uses iron oxide and nickel oxide, the loading of...
Embodiment 2
[0031] A kind of preparation method for high activity fluid bed catalyst is as follows:
[0032] 1) Soak the zeolite molecular sieve in 1mol / L alkali solution for 20min, then wash it with distilled water for 5 times, and let it dry naturally;
[0033] 2) Soak the zeolite molecular sieve in step 1) in the dilute solution of ferric nitrate and nickel nitrate, coat by dipping and pulling, then burn at 400°C for 2-3 hours, and cool naturally;
[0034] 3) Soak the zeolite molecular sieve coated with the metal oxide catalyst in step 2) in the platinum-doped alumina nanosuspension, coat the film by dipping and pulling, burn at 200°C for 2 hours, and cool naturally;
[0035] 4) Soak the zeolite molecular sieve in step 3) in molybdenum nitrate solution, pull the coating, burn at 300°C for 1 hour, and cool naturally;
[0036] 5) Put the zeolite molecular sieve prepared in step 4) into a muffle furnace for gradient high-temperature burning, burning at 200°C for 2 hours, burning at 400°C...
Embodiment 3
[0041] A kind of preparation method for high activity fluid bed catalyst is as follows:
[0042] 1) Soak the zeolite molecular sieve in 1mol / L alkali solution for 20min, then wash it with distilled water for 5 times, and let it dry naturally;
[0043] 2) Soak the zeolite molecular sieve in step 1) in the dilute solution of ferric nitrate and nickel nitrate, coat the film by dipping and pulling, then burn at 500°C for 2-3 hours, and cool naturally;
[0044] 3) Soak the zeolite molecular sieve coated with the metal oxide catalyst in step 2) in the platinum-doped alumina nanosuspension, coat the film by dipping and pulling, burn at 300°C for 2 hours, and cool naturally;
[0045] 4) Soak the zeolite molecular sieve in step 3) in molybdenum nitrate solution, pull the coating, burn at 300°C for 1 hour, and cool naturally;
[0046] 5) Put the zeolite molecular sieve prepared in step 4) into a muffle furnace for gradient high-temperature burning, burning at 200°C for 2 hours, burning...
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