Azo compound dye and preparation method thereof

A dye and azo technology, which is applied in the field of azo composite dyes and its preparation, can solve problems such as unstable properties and damage, and achieve the effect of improving stability

Inactive Publication Date: 2016-10-12
无锡润新染料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional azo dyes are unstable, and will decompose a variety of carcinogenic aromatic hydroc

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] 80 parts of azobisisobutyronitrile, 30 parts of m-phenylenediamine, 40 parts of sodium lauryl sulfate, 20 parts of monoglyceride, 10 parts of p-methylaniline, 10 parts of curing agent Import into the reaction kettle and heat to 80 degrees Celsius, stir and mix for 30 minutes; continue to add 120 parts of water to the reaction kettle, keep stirring, and continue for 10 minutes; pass the resulting mixture through a cold water bath below 5 degrees Celsius; finally filter the mixture , collect the crystals, put them aside for 1 to 2 days, and pack them into the warehouse.

Embodiment 2

[0016] 100 parts by mass of azobisisobutyronitrile, 40 parts of m-phenylenediamine, 60 parts of sodium lauryl sulfate, 30 parts of monoglyceride, 30 parts of p-methylaniline, 30 parts of curing agent Import into the reaction kettle and heat to 80 degrees Celsius, stir and mix for 40 minutes; continue to add 150 parts of water to the reaction kettle, keep stirring, and continue for 20 minutes; pass the resulting mixture through a cold water bath below 5 degrees Celsius; finally filter the mixture , collect the crystals, put them aside for 1 to 2 days, and pack them into the warehouse.

Embodiment 3

[0018] With 90 parts of azobisisobutyronitrile, 35 parts of m-phenylenediamine, 50 parts of sodium lauryl sulfate, 25 parts of monoglyceride, 20 parts of p-methylaniline, 20 parts of curing agent Import into the reaction kettle and heat to 80 degrees Celsius, stir and mix for 35 minutes; continue to add 130 parts of water to the reaction kettle, keep stirring, and continue for 15 minutes; pass the resulting mixture through a cold water bath below 5 degrees Celsius; finally filter the mixture , collect the crystals, put them aside for 1 to 2 days, and pack them into the warehouse.

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PUM

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Abstract

The invention discloses an azo composite dye, which comprises the following components in parts by mass: 80-100 parts of azobisisobutyronitrile, 30-40 parts of m-phenylenediamine, and 40-60 parts of dodecanol Sodium sulfate, 20~30 parts of monoglyceride, 10~30 parts of p-methylaniline, 10~30 parts of curing agent and 120~150 parts of water. At the same time, the invention also discloses a preparation method of the azo composite dye. Compared with the traditional technology, the present invention improves the stability of the azo composite dye by adding highly stable organic aromatic hydrocarbon groups and low-temperature modification treatment, and avoids the decomposition of various carcinogenic aromatic hydrocarbons due to environmental influences in the later stage.

Description

technical field [0001] The invention belongs to the field of dye synthesis, and in particular relates to an azo composite dye and a preparation method thereof. Background technique [0002] A class of organic compounds in which the azo groups of azo dyes are connected to aryl groups at both ends are the most widely used synthetic dyes in the printing and dyeing process of textiles and clothing. They are used for dyeing and printing of various natural and synthetic fibers, and are also used for paints. , plastic, rubber and other coloring. Traditional azo dyes are unstable in nature, and will decompose a variety of carcinogenic aromatic hydrocarbons under certain conditions, causing considerable harm to the environment and the human body. Contents of the invention [0003] Purpose of the invention: the purpose of the present invention is to provide a kind of azo complex dye for the deficiencies in the prior art. [0004] Another object of the present invention is to provi...

Claims

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Application Information

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IPC IPC(8): C09B67/22
CPCC09B67/0041
Inventor 周佳易
Owner 无锡润新染料有限公司
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