A preparation method of high and low temperature resistant micro-nano lubricating material
A kind of lubricating material, high and low temperature resistant technology, used in lubricating compositions, petroleum industry and other directions, can solve the problems of poor lubricating performance, loss of lubricating performance, easy aggregation and growth, etc., to achieve long service life, prolong service life, friction coefficient low effect
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example 1
[0017]First, weigh 180g of cobalt nitrate and 240g of ferric nitrate successively, add them into a beaker containing 1200mL of deionized water, stir with a glass rod until they are completely dissolved, then pour the solution in the beaker into a crucible, heat, evaporate and crystallize, and wait for it to cool naturally to At room temperature, transfer the crystals in the crucible to a ball mill, then add 45g of urea, add ball milling beads according to the ball-to-material ratio of 3:1, ball mill at a speed of 380r / min for 15min, discharge the material, and transfer the obtained material to an oven at 105°C. Dry to constant weight to obtain mixed crystal powder, and set aside; measure 3L biogas liquid, transfer it to a refrigerator at 2°C, refrigerate for 16 hours, pour it into a receiving tank, set aside; take two bottles of oxygen, and the pressure of No. 1 oxygen bottle is 0.4MPa, the pressure of the No. 2 oxygen cylinder is 0.5MPa, the No. 2 oxygen cylinder and the 0.11M...
example 2
[0020] First, weigh 190g of cobalt nitrate and 250g of ferric nitrate in sequence, add them into a beaker containing 1400mL of deionized water, stir with a glass rod until they are completely dissolved, then pour the solution in the beaker into a crucible, heat, evaporate and crystallize, and wait for it to cool naturally to At room temperature, transfer the crystals in the crucible to a ball mill, then add 53g of urea, add ball milling beads according to the ball-to-material ratio of 3:1, ball mill at a speed of 420r / min for 17min, discharge the material, and transfer the obtained material to an oven at 107°C. Dry to constant weight to obtain mixed crystal powder, and set aside; measure 4L biogas liquid, transfer it to a 3°C refrigerator, refrigerate for 20 hours, pour it into a receiving tank, set aside; take two bottles of oxygen, and the pressure of No. 1 oxygen bottle is 0.5MPa, the pressure of the No. 2 oxygen cylinder is 0.6MPa, the No. 2 oxygen cylinder and the 0.12MPa ...
example 3
[0023] First, weigh 200g of cobalt nitrate and 260g of ferric nitrate in sequence, add them into a beaker containing 1600mL of deionized water, stir with a glass rod until they are completely dissolved, then pour the solution in the beaker into a crucible, heat, evaporate and crystallize, and wait for it to cool naturally to At room temperature, transfer the crystals in the crucible to a ball mill, then add 60g of urea, add ball milling beads according to the ball-to-material ratio of 3:1, ball mill at a speed of 460r / min for 20min, discharge the material, and transfer the obtained material to an oven at 110°C. Dry to constant weight to obtain mixed crystal powder, and set aside; measure 5L biogas liquid, transfer it to 4°C refrigerator, refrigerate for 24 hours, pour it into the receiving tank, set aside; take two bottles of oxygen, the pressure of No. 1 oxygen bottle is 0.6MPa, the pressure of the No. 2 oxygen cylinder is 0.7MPa, the No. 2 oxygen cylinder and the 0.13MPa acet...
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