A kind of preparation method of functional polymer material

A technology of functional polymers and polymer materials, applied in the field of preparation of functional polymer materials, can solve problems such as low efficacy and high cost, and achieve the effects of improving efficacy, easy promotion, and reducing dosage

Active Publication Date: 2018-07-20
WUYI UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to solve the disadvantages of low efficiency and high cost of functionalization of traditional polymer materials through blending and surface chemical grafting, and to provide a preparation method for functional polymer materials. The present invention acts on functional substances through alternating electric fields Particles, so that they are physically embedded in the surface of the softened polymer material substrate, and chemically cross-linked with the surface of the polymer material substrate. After the polymer material substrate is cured, the functional polymer material can be obtained

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] What this embodiment 1 describes is the preparation of antibacterial and anti-mite hygroscopic polyester fiber, and its specific preparation method is as follows:

[0029] (1) Mix zinc sulfide powder with an average particle size of 200 nm and zircoaluminate coupling agent at a mass ratio of 1:0.05, and spray the mixed substance particles onto the negative electrode of a DC electric field at a speed of 50 g / min , the electric field voltage is 10,000 volts, and the frequency of changing the direction of the positive and negative electrodes is 20 Hz. The electric field accelerates the mixture of zinc sulfide powder and acrylamide monomer. When the mixture moves at a high speed to the middle of the positive and negative electrode plates, the electrode direction is constantly changed. , so that the mixture moves back and forth at high speed in the middle of the electrode, forming a concentrated dynamic equilibrium mixture particle cloud;

[0030] (2) The polyester spinning ...

Embodiment 2

[0032] This embodiment 2 describes the preparation of cordycepin molecularly imprinted polypropylene fiber, and its specific preparation method is as follows:

[0033](1) Spray the molecularly imprinted powder of cordycepin with an average particle size of 700 nm onto the negative electrode of a DC electric field at a speed of 60 g / min. The electric field voltage is 50,000 volts, and the positive and negative electrodes change direction The frequency is 40 Hz, and the electric field accelerates the nano-cordycepin molecularly imprinted powder. When the cordycepin molecularly imprinted powder moves to the middle of the positive and negative electrode plates at high speed, the direction of the electrode is constantly changed, so that the nano-cordycepin molecularly imprinted powder is in the middle of the electrode. High-speed movement back and forth to form a concentrated dynamic equilibrium nano-cordycepin molecularly imprinted powder cloud;

[0034] (2) The polypropylene spin...

Embodiment 3

[0036] What present embodiment 3 describes is the preparation of icy viscose fiber, and its specific preparation method is as follows:

[0037] (1) The icy jade powder with an average particle size of 2 um and the polymethylsiloxane coupling agent are mixed at a mass ratio of 1:0.01, and the mixed substance particles are sprayed into the DC electric field at a speed of 150 g / min. On the negative electrode, the electric field voltage is 100,000 volts, and the frequency of changing direction of the positive and negative electrodes is 50 Hz. The electric field accelerates the icy jade powder, and when the icy jade powder moves to the middle of the positive and negative electrode plates at high speed, the electrodes are constantly changed. Direction, so that the icy jade powder moves back and forth at high speed in the middle area of ​​the electrode, forming a concentrated and dynamically balanced cloud of nano icy jade powder;

[0038] (2) The cellulose spinning solution is extru...

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Abstract

The invention discloses a preparation method of a functional polymer material, which belongs to the field of fiber material and plastic processing. The purpose of the present invention is to solve the disadvantages of low efficiency and high cost of functionalization of traditional polymer materials through blending and surface chemical grafting. The present invention acts on the functional material particles through an alternating electric field to physically embed them into the softened extrusion molding The surface of the polymer material substrate, and make the crosslinking group and the surface of the polymer material substrate realize chemical crosslinking and physical blending. After the polymer material substrate is cooled and solidified by cold wind or stretched, it will The functional polymer material can be obtained. The functional substances in the method of the present invention have a wide selection range, high utilization rate, good efficacy, less dosage, short material preparation process and high efficiency, and can be widely used in textile and garment industries, plastic industries, environmental governance and drug extraction, etc. field.

Description

technical field [0001] The invention belongs to the field of fiber material and plastic processing, and in particular relates to a preparation method of a functional polymer material. Background technique [0002] At present, there are mainly two methods for preparing functional materials: blending modification and surface chemical grafting modification. One is the blending modification method, which directly molds functional substances and polymer solutions or melts. The prepared functional material, whose functional components are completely embedded in the polymer material, not only cannot exert its functional effect, but also consumes a large amount of functional substances, which greatly increases the cost, and even causes difficulty in molding due to the mixing of functional components; The second is the surface grafting modification method, which generates free radicals on the surface through irradiation and other methods, and then grafts functional substance monomers...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F11/08D01F11/06D01F11/02D01D5/08C08J3/24C08L27/06B29C59/00
CPCB29C48/002C08J3/24C08J2327/06D01D5/08D01F11/02D01F11/06D01F11/08
Inventor 巫莹柱
Owner WUYI UNIV
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