A kind of dyeing process of red vegetable dye
A technology of red plants and dyes, applied in the field of dyeing technology, which can solve the problems of reducing the purity of red pigment, incapable of large-scale production, and perishable red pigment, so as to improve the extraction efficiency and extraction amount, facilitate understanding and operation, and simplify the process flow Effect
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Embodiment 1
[0028] Example 1. A kind of dyeing process of red vegetable dye, comprises the following steps:
[0029] a. Soak the safflower cake in an acetic acid solution with a pH value of 5-6 for 60-70 minutes, filter to obtain the A safflower cake, and then decoct the A safflower cake with ebony water at a temperature of 50°C-60°C for 100-150 minutes Minutes to obtain the mixed solution A1 of A safflower cake and ebony water, and then heat the mixed solution A1 to 80℃-90℃ at a speed of 2°C / min-4°C / min, and then continue to decoct for 150-200 minutes to obtain the mixed solution A2, the mixture A2 is filtered and cooled to obtain filter residue A; after multiple treatments, the yellow pigment in the safflower cake can be effectively removed and the purity of the red pigment can be improved.
[0030] b. Put the filter residue A in a plant ash solution with a pH value of 9-11 and a temperature of 25°C-40°C for rinsing for 40-50 minutes, and filter to obtain the dye liquor B1 and filter r...
Embodiment 2
[0051] Example 2. A kind of dyeing process of red vegetable dye, comprises the following steps:
[0052] a. Soak the safflower cake in an acetic acid solution with a pH value of 5 for 60 minutes, filter to obtain A safflower cake, and then decoct A safflower cake in ebony water at a temperature of 50°C for 100 minutes to obtain A safflower cake and ebony Mixed solution A1 of water, then heated mixed solution A1 to 80°C at a rate of 2°C / min and continued to decoct for 150 minutes to obtain mixed solution A2, which was filtered and cooled to obtain filter residue A;
[0053] b. Put the filter residue A into a plant ash solution with a pH value of 9 and a temperature of 25°C for rinsing for 40 minutes, filter to obtain the dye solution B1 and filter residue b1; put the filter residue b1 into a plant ash solution with a pH value of 9 and a temperature of 50°C Rinse in the solution for 20 minutes, filter to obtain dye liquor B2 and filter residue b2; put filter residue b2 into a p...
Embodiment 3
[0072] Example 3. A kind of dyeing process of red vegetable dye, comprises the following steps:
[0073] a. Soak the safflower cake in an acetic acid solution with a pH value of 6 for 70 minutes, filter to obtain A safflower cake, then decoct A safflower cake in ebony water at a temperature of 60°C for 150 minutes to obtain A safflower cake and ebony Mixed solution A1 of water, then heated mixed solution A1 to 80°C-90°C at a rate of 4°C / min and then continued to decoct for 200 minutes to obtain mixed solution A2, which was filtered and cooled to obtain filter residue A;
[0074] b. Put the filter residue A into a plant ash solution with a pH value of 11 and a temperature of 40°C for rinsing for 50 minutes, and filter to obtain the dye solution B1 and filter residue b1; put the filter residue B1 into a plant ash solution with a pH value of 11 and a temperature of 60°C Rinse in the solution for 30 minutes, filter to obtain dye liquor B2 and filter residue b2; put filter residue...
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