Staged-temperature-controlled reactor and stirring shaft thereof
A sectioned temperature control and reactor technology, applied in the field of reactors, can solve the problems of complex structures of reactors and agitators, difficult to ensure adequate mixing, and increase heat exchange load, etc., to achieve good heat exchange effect and increase disturbance effect. , the effect of promoting secondary flow
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Embodiment 1
[0045] Such as figure 2 , Figure 4 As shown, a segmented temperature control reactor, the first chamber 121 is close to the feed port 21, the second chamber 122 is close to the discharge port 23, and there are two jackets 3 on the outside of the cavity 2, which are different from the first The chamber 121 corresponds to the first jacket 31 , and the second chamber 122 corresponds to the second jacket 32 . The two jackets 3 are independent of each other and act on the upper and lower sections of the cavity 2 respectively.
[0046] A heat medium flows in the first chamber 121 and the first jacket 31 respectively, and a cold medium flows in the second chamber 122 and the second jacket 32 , and acts on both ends of the cavity 2 to exchange heat for the material. Timely changes and adjustments are made according to the different requirements of exothermic and endothermic reactions to ensure the effect of temperature changes in the continuous production process and solve the ...
Embodiment 2
[0053] The same part as Embodiment 1 will not be repeated, such as Figure 7 As shown, a third jacket 33 is provided between the first jacket 31 and the second jacket 32 , and the three jackets 3 are independent of each other and act on the upper, middle and lower positions of the cavity 2 respectively.
[0054] A heat medium flows in the first chamber 121 and the first jacket 31 respectively, a cold medium flows in the second chamber 122 and the third jacket 33 respectively, and a heat medium flows in the second jacket 32 .
[0055] The heat exchange flow process of embodiment two:
[0056] The reaction materials enter the cavity 2 through different feeding ports 21 and feeding chambers 22 respectively, and at the same time, the stirring shaft 1 stirs to accelerate the mixing of the reaction materials. The first chamber 121 and the coiled pipe 13 and the first jacket 31 The conditions required to establish the reaction temperature of the material on both sides of the mat...
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