A kind of sludge activated carbon anaerobic granular sludge and preparation method thereof
A technology of anaerobic granular sludge and sludge activated carbon, which is applied in water/sludge/sewage treatment, anaerobic digestion treatment, chemical instruments and methods, etc., can solve the problem of high cost of activated carbon, and achieve low raw material cost and stable structure , Improve the effect of purification ability
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Embodiment 1
[0022] (1) Dry the sludge particles, grind them into powder, and mix with Fe 3 o 4 Mix the powder, add the mixed powder to 4mol / LZnCl 2 solution, stir evenly, after ultrasonication for 40min, activate at 70°C for 36h, then dry the sludge powder, add deionized water and stir evenly, press into the model, and then put it in the muffle furnace at 480 ℃ calcination for 3 hours to obtain magnetic sludge activated carbon;
[0023] (2) The magnetic sludge activated carbon prepared in the previous step is ground into powder, added to common anaerobic activated sludge and cultivated, the feeding amount of magnetic sludge activated carbon is 300g, in the anaerobic activated sludge reactor For cultivation, the volume of the reactor is 300L, the ordinary anaerobic activated sludge inoculated accounts for 30% of the volume of the reactor, the temperature condition is 18-28°C, the COD in the daily influent is 2000mg / L, the influent is 12L, and the residence time For 18 hours, sludge acti...
Embodiment 2
[0026] (1) Dry the sludge particles, grind them into powder, and mix with Fe 3 o 4 Mix the powder, add the mixed powder to 5mol / LZnCl 2 solution, stir evenly, after ultrasonication for 50min, activate at 70°C for 36h, then dry the sludge powder, add deionized water and stir evenly, press into the model, and then put it in the muffle furnace at 630 Calcined at ℃ for 4h to prepare magnetic sludge activated carbon;
[0027] (2) The magnetic sludge activated carbon prepared in the previous step is ground into powder and added to common anaerobic activated sludge for cultivation. For cultivation, the volume of the reactor is 300L, the ordinary anaerobic activated sludge inoculated accounts for 30% of the volume of the reactor, the temperature condition is 18-28°C, the COD in the daily influent is 3000mg / L, the influent is 12L, and the residence time For 18 hours, sludge activated carbon anaerobic granular sludge was prepared.
[0028] The sludge activated carbon anaerobic granu...
Embodiment 3
[0030] (1) Dry the sludge particles, grind them into powder, and mix with Fe 3 o 4 Mix the powder, add the mixed powder to 6mol / LZnCl 2 solution, stir evenly, after ultrasonication for 30min, activate at 65°C for 36h, then dry the sludge powder, add deionized water to stir evenly, press into the model, and then put it in the muffle furnace at 550 Calcined at ℃ for 4h to prepare magnetic sludge activated carbon;
[0031] (2) The magnetic sludge activated carbon prepared in the previous step is ground into powder, added to common anaerobic activated sludge and cultivated, the feeding amount of magnetic sludge activated carbon is 600g, in the anaerobic activated sludge reactor For cultivation, the volume of the reactor is 300L, the ordinary anaerobic activated sludge inoculated accounts for 30% of the volume of the reactor, the temperature condition is 18-28°C, the COD in the daily influent is 4000mg / L, the influent is 12L, and the residence time For 18 hours, sludge activated...
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