Composite shape-setting phase change material and preparation method thereof
A shape-setting phase-change material and a technology for phase-change materials, which are applied in the field of composite shape-setting phase-change materials and their preparation, can solve problems such as poor thermal stability, and achieve the effects of reducing phase separation, a simple and convenient preparation method, and broad application prospects.
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[0032] Step 1: Acid treatment of sepiolite
[0033] Sepiolite and hydrochloric acid (0.1 mol / L) were mixed with a solid-to-liquid ratio of 1:20, ultrasonicated and stirred for 1 hour, then left to stand for 12 hours to remove the quartz impurities at the bottom, washed repeatedly until neutral, suction filtered, dried, grind.
[0034] Step 2: High temperature treatment of sepiolite
[0035] Put the sepiolite obtained in step 1 into the muffle furnace, 420 o C activated for 2 h.
[0036] Step 3: Organic treatment of sepiolite
[0037] The 5g sepiolite that step 2 obtains is configured into the suspension of 20 g / L, pours in the three-necked flask, 50 o C preheat for 15 min. Mix and shake 2 ml KH570 (1% mass fraction) with 100 ml ethanol solution (95% mass fraction) for 30 minutes to obtain the silane coupling agent hydrolyzate into a three-necked flask, then add sodium hexametaphosphate (7 mass fraction %) as a dispersant, 95 o C was refluxed and condensed for 2 h, and f...
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