A preparation method of biomass-based nitrogen-containing porous carbon, porous carbon and its application
A biomass and porous carbon technology, which is applied in the preparation/purification of carbon, chemical instruments and methods, carbon compounds, etc., can solve the problems of large amount of use, complicated synthesis process, and high cost, and achieve high rate performance, environmental friendliness, The effect of easy operation
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[0030] The preparation method of the nitrogen-doped porous carbon material according to the present invention is a hydrothermal method, and the porous nitrogen-doped carbon material synthesized by this method has a large specific surface area and abundant micro-mesoporous structure. The method uses renewable protein-rich biomass as raw material, without adding nitrogen source, to prepare nitrogen-doped porous carbon material in situ in one step, and the porous nitrogen-containing material has excellent electric double layer capacitance performance and good cycle stability.
[0031] Alkali is used as an activator in the chemical activation method of the prior art, but in order to make the final activated carbon product have sufficient micropore or mesoporous structure, it is often necessary to use a large amount of alkali as an activator, and the activator is usually doubled, or even several times the amount of biomass raw material. In comparison, the present invention adopts ...
Embodiment 1
[0037] 1 kg of cleaned bamboo shoots was cut into pieces, heated to dryness in an oven at 70° C., and the obtained solid was ground into powder. Take 2g of powder and add it to 20mL of dilute sulfuric acid with a weight percentage of 0.5%, stir and mix evenly, then move to a hydrothermal reaction kettle, react at 210°C for 12 hours, filter, wash, and dry to obtain a brown solid. Afterwards, the obtained dried solid was calcined in a tube furnace in a nitrogen gas atmosphere, and kept at 800° C. for 8 hours. After the tube furnace dropped to room temperature, the sample was taken out to obtain a nitrogen-doped porous carbon material with a nitrogen content of about 2.9% and a specific surface area of 1893m 2 / g. figure 1 and figure 2 It is the BET and SEM result figure of the nitrogen-doped porous carbon material prepared according to the present embodiment, such as figure 1 and figure 2 As shown by the data, the material contains a well-developed micro- and meso-porous...
Embodiment 2
[0039] 1 kg of cleaned bamboo shoots was cut into pieces, heated to dryness in an oven at 70° C., and the obtained solid was ground into powder. Take 2g of powder and add it to 20mL of water (without adding acid), stir and mix evenly, then move to a hydrothermal reaction kettle, react at 210°C for 12 hours, filter, wash, and dry to obtain a brown solid. Afterwards, the obtained dried solid was calcined in a tube furnace in a nitrogen gas atmosphere, and kept at 900° C. for 8 hours. After the tube furnace dropped to room temperature, the sample was taken out to obtain a nitrogen-doped porous carbon material with a specific surface area of 935m 2 / g, the nitrogen content is 1.7%.
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