Disperse dye paste capable of effectively retarding precipitation and preparation method

A technology for disperse dyes and sizing, applied in organic dyes, dyeing methods, textiles and papermaking, etc., can solve the problems of decreased stability of dye colloidal suspension, difficult to uniformly disperse dye particles, larger particles, etc., to improve storage stability Good properties, excellent dyeing and finishing fastness, and the effect of reducing the average particle size

Active Publication Date: 2017-05-24
ZHEJIANG DIBANG CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that the dyes are obviously aggregated, the particles are obviously larger, and the average particle size is also greatly improv

Method used

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  • Disperse dye paste capable of effectively retarding precipitation and preparation method
  • Disperse dye paste capable of effectively retarding precipitation and preparation method
  • Disperse dye paste capable of effectively retarding precipitation and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Example

[0055] Examples 1~3

[0056] Without adding urea, select disperse dyes and dispersants to grind, and then adjust them into disperse dye finished slurry. The experimental data is according to Table 1:

[0057] Table 1

[0058]

[0059] Precipitation effect detection

[0060] The disperse dye slurries prepared in the above Examples 1 to 3 were allowed to stand for a certain period of time, and then the sedimentation degree was tested according to the method described above. The results are shown in Table 2:

[0061] Table 2

[0062] Example Precipitation % / 7 days Precipitation % / 30 days Precipitation % / 60 days

[0063] 145.4980.1783.17 230.5267.3373.43 318.0454.6468.54

[0064] It can be seen from the test results in Table 2 that the amount of dispersant has a significant effect on the precipitation rate of the disperse dye slurry. As the amount of dispersant increases, the degree of precipitation decreases and the precipitation of the slurry slows down significantly. In addition,...

Example

[0065] Examples 4-9

[0066] Without urea, select disperse dyes and dispersants after grinding, adjust the pH value of the slurry with phosphoric acid to make the finished disperse dye slurry. The experimental data is according to Table 3:

[0067] table 3

[0068]

[0069] Precipitation effect detection

[0070] The disperse dye slurries prepared in the foregoing Examples 4-9 were allowed to stand for a certain period of time, and then the degree of precipitation was tested according to the method described above. The results are shown in Table 4:

[0071] Table 4

[0072] Example Precipitation % / 7 days Precipitation % / 30 days Precipitation % / 60 days 444.7881.6883.94 540.1882.2184.46 639.1579.3982.65 743.4680.1485.15 846.1884.8686.33 948.8585.288.32

[0073] The pH value of the finished disperse dye slurry is generally 7-8. Too high or too low will affect the storage performance and use performance of the slurry. From the sedimentation test results in Table 4, it can be seen that t...

Example

[0074] Examples 10-17

[0075] The disperse dye, dispersant, and urea are mixed and ground to prepare a finished disperse dye slurry. The experimental data is based on Table 5:

[0076] table 5

[0077]

[0078]

[0079] Precipitation effect detection

[0080] The disperse dye slurries prepared in the above Examples 10-17 were allowed to stand for a certain period of time, and then the sedimentation degree was tested according to the method described above. The results are shown in Table 6:

[0081] Table 6

[0082] Example Precipitation % / 7 days Precipitation % / 30 days Precipitation % / 60 days 1043.8379.8586.04 1139.8978.9685.81 1235.4177.6585.13 1326.2176.9684.8 1425.1371.2282.27 1521.3764.6679.12 167.8546.8376.42 176.5840.1675.18

[0083] It can be seen from the sedimentation test results in Table 6 that as the amount of urea increases, the sedimentation rate of the disperse dye product slurry is significantly slowed down, and the higher the amount of urea, the slower the sediment...

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PUM

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Abstract

The invention discloses a disperse dye paste capable of effectively retarding precipitation. The disperse dye paste is characterized by comprising urea with a weight of 0.05 to 0.5 time of the total weight of a disperse dye component, and a dispersant with a weight of 0.6 to 6 times of the total weight of the disperse dye component, wherein the disperse dye component is one or more selected from compounds as shown in a formula in the specification. In the formula, R1 is H or -NO2; R2 and R3 are selected from the group consisting of H, or -Cl, -Br, -CN, -CF3, -NO2 and -COOR8; R4 and R5 are selected from the group consisting of H, or alkyl, alkoxy and -NHCOR9; R6 and R7 are selected from the group consisting of alkyl, alkoxy, or alkyl or alkoxy with an H substituted by -OH, -CN or -Ph; and R8 and R9 are alkyl. The disperse dye provided by the invention is a liquid dye, and has high dyeing rate, good deep dyeing properties and excellent dyeing fastness; and compared with an ordinary commercial disperse dye paste, the disperse dye paste provided by the invention has the following advantages: the aggregation and precipitation rate of dye particles is significantly reduced, and better storage stability is obtained.

Description

technical field [0001] The invention belongs to the technical field of dye synthesis, and in particular relates to a disperse dye slurry which can effectively slow down precipitation and a preparation method. Background technique [0002] As the output of synthetic fibers increases year by year, disperse dyes are currently one of the most rapidly developing dyes. At present, the finished products of disperse dyes mainly come in two forms: dry powder and liquid slurry, and liquid slurry has limited its wide-scale application and promotion due to problems such as high transportation cost and easy deterioration of slurry. [0003] The main reasons why the liquid finished product slurry of disperse dyes are easy to deteriorate after storage are as follows: [0004] First of all, during the placement process, the dye will become mildewed or deteriorated, the dye or the surface of the dye will be oxidized, the molecular structure of the dye will change, and thus the shade of the ...

Claims

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Application Information

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IPC IPC(8): C09B67/38C09B67/10C09B67/04D06P1/18
Inventor 徐万福傅伟松周乃锋唐智勇陈华祥叶勤刚
Owner ZHEJIANG DIBANG CHEM
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