Coating adhesive for polyester clean clothes fabric and preparation method thereof
A technology of clean clothes and coating glue, which is applied in fiber treatment, textile and papermaking, biochemical fiber treatment, etc., to achieve excellent washing resistance, enhanced film-forming performance, and improved dust filterability
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Embodiment 1
[0027] Add the polybutadiene glycol 50 of the Polyethylene Glycol 10 of MDI 50, the Polyethylene Glycol 10 of average molecular weight 1450, the Polyethylene Glycol 15 of average molecular weight 1000, the average molecular weight 2000 of diphenylmethane diisocyanate (MDI) 50, the average molecular weight, and heat up to 75°C, react for 2.5 hours, then cool down to 50°C, add styrene 10, neoprene 10, methacryloyloxyethyltrimethylammonium chloride 5, deionized water 150, heat up to 75°C, drop A mixed solution containing initiator 2,2'-azobisisobutylamidine dihydrochloride 1 and deionized water 10 was added dropwise in 2 hours, then kept at 80°C for 1 hour, cooled to 45°C and discharged to obtain Acrylic modified polyurethane emulsion;
[0028] The acrylic modified polyurethane emulsion 100 prepared above was added to the polyurethane leveling rheological agent 2 and the blocked isocyanate crosslinking agent 2, stirred evenly, and filtered to obtain the product, the product visco...
Embodiment 2
[0030] Add the polybutadiene glycol 55 of the Polyethylene Glycol 12 of 60, the Polyethylene Glycol 12 of average molecular weight 1450, the Polyethylene Glycol 16 of average molecular weight 1000, the average molecular weight 2000 of diphenylmethane diisocyanate (MDI) 60, average molecular weight, heat up to 70°C, react for 2.6 hours, then cool down to 55°C, add styrene 12, neoprene 15, methacryloyloxyethyltrimethylammonium chloride 6, deionized water 180, heat up to 70°C, drop A mixed solution containing initiator 2,2'-azobisisobutylamidine dihydrochloride 1.5 and deionized water 15 was added dropwise in 2.2 hours, then kept at 81°C for 1 hour, cooled to 45°C and discharged to obtain Acrylic modified polyurethane emulsion;
[0031] The acrylic modified polyurethane emulsion 100 prepared above was added to the polyurethane leveling rheology agent 3 and the blocked isocyanate crosslinking agent 2.5, stirred evenly, and filtered to obtain the product, the product viscosity was ...
Embodiment 3
[0033] Add the polybutadiene glycol 58 of the Polyethylene Glycol 14 of 65, the Polyethylene Glycol 14 of average molecular weight 1450, the Polyethylene Glycol 18 of average molecular weight 1000, the average molecular weight 2000 of diphenylmethane diisocyanate (MDI) 65, average molecular weight into reaction kettle, be heated up to 78°C, react for 2.8 hours, then cool down to 56°C, add styrene 16, neoprene 17, methacryloyloxyethyltrimethylammonium chloride 8, deionized water 190, heat up to 78°C, drop A mixed solution containing initiator 2,2'-azobisisobutylamidine dihydrochloride 1.8 and deionized water 18 was added dropwise in 2.3 hours, then kept at 83°C for 1 hour, cooled to 45°C and discharged to obtain Acrylic modified polyurethane emulsion;
[0034] The acrylic-modified polyurethane emulsion 100 prepared above was added to the polyurethane leveling rheological agent 4 and the blocked isocyanate crosslinking agent 3, stirred evenly, and filtered to obtain the product ...
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