A kind of super heat insulation airgel foam concrete and preparation method thereof
A technology of foam concrete and airgel, which is applied in the field of light weight, heat insulation, fire prevention and sound insulation materials, and can solve the problems of the decline of the mechanical properties of foam concrete, the shedding of airgel powder, and the difficulty of uniform distribution of airgel, etc.
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[0026] A preparation method of super heat-insulating aerogel foam concrete includes the following steps:
[0027] (1) Modification of aerogel powder;
[0028] (2) Dry mix the aerogel powder obtained in step (1) with the gelling material, and then add water to wet mix;
[0029] (3) Mix and stir the wet mixture obtained in step (2) with the prefabricated foam.
[0030] In addition, step (2) of the present invention can also be dry blending the gelling material, then adding water to wet blending, and adding the aerogel powder obtained in step (1) during wet blending.
[0031] In this way, the preparation method of the aerogel foam concrete of the present invention has the advantages of simple process, short process cycle, waste and environmental protection, etc., and is very suitable for industrial production.
[0032] In this embodiment, the step (1) includes a hydrophobic modification step; the hydrophobic modification step is to hydrophobically modify the aerogel powder in a closed hydro...
Embodiment 1
[0050] Use the following steps to prepare SiO 2 Aerogel foam concrete:
[0051] (1) Use a contact angle measuring instrument to detect the SiO to be processed 2 The contact angle between the surface of the aerogel powder and water, the test result is 55°, and the SiO with a particle size of 56μm 2 The aerogel powder is placed in a vacuum heating furnace, and the weighed hexamethyldisilazane is placed in a vacuum heating furnace with a container, heated and gasified, and hydrophobically modified for 1.5 hours to obtain hydrophobic SiO 2 Aerogel powder, use a contact angle measuring instrument to detect hydrophobic SiO 2 The contact angle between the surface of the aerogel powder and water is 147°;
[0052] (2) At room temperature, weigh ethanol, n-hexane, and deionized water at a mass ratio of 1:1:100, mix them evenly, and prepare a surface hydrophilic modification solution;
[0053] (3) Press hydrophobic SiO 2 The volume ratio of the aerogel powder and the surface hydrophilic modifica...
Embodiment 2
[0062] Use the following steps to prepare SiO 2 Aerogel foam concrete:
[0063] (1) Use a contact angle measuring instrument to detect the SiO to be processed 2 The contact angle between the surface of the aerogel powder and water, the test result is 45°, and the SiO with a particle size of 0.1mm 2 The aerogel powder is placed in a vacuum heating furnace, and the weighed trimethylchlorosilane is placed in a vacuum heating furnace with a container, heated and gasified, and hydrophobically modified for 1.5 hours to obtain hydrophobic SiO 2 Aerogel powder, use a contact angle measuring instrument to detect hydrophobic SiO 2 The contact angle between the surface of the aerogel powder and water is 146°;
[0064] (2) At room temperature, weigh the fatty alcohol polyoxyethylene ether ammonium sulfate, n-hexane, acetone and deionized water at a mass ratio of 1:0.4:0.4:130, mix them evenly, and configure the surface hydrophilic modification solution;
[0065] (3) Press hydrophobic SiO 2 The vo...
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