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A kind of super heat insulation airgel foam concrete and preparation method thereof

A technology of foam concrete and airgel, which is applied in the field of light weight, heat insulation, fire prevention and sound insulation materials, and can solve the problems of the decline of the mechanical properties of foam concrete, the shedding of airgel powder, and the difficulty of uniform distribution of airgel, etc.

Active Publication Date: 2020-02-18
NANJING WEICAI NEW ENERGY TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] However, the following technical bottlenecks are encountered in the research and development of airgel foam concrete: (1) Due to the large difference in density between airgel powder and concrete, during the mixing process, phase separation between the two is easy to occur, resulting in air condensation It is difficult for the glue to be evenly distributed in the concrete system, resulting in a serious decline in the mechanical properties of the foamed concrete, and the improvement of the thermal insulation performance is not obvious; (2) During the preparation of the foamed concrete, the airgel nanoporous structure is easily destroyed by water and cement in the concrete The additives in the raw materials are destroyed, and the excellent thermal insulation performance of the airgel due to the nanoporous structure characteristics is lost; (3) The mechanical properties of the foam concrete are significantly reduced due to the low interface strength between the airgel and the cementitious material. And it is easy to cause the airgel powder to fall off from the concrete matrix

Method used

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  • A kind of super heat insulation airgel foam concrete and preparation method thereof
  • A kind of super heat insulation airgel foam concrete and preparation method thereof
  • A kind of super heat insulation airgel foam concrete and preparation method thereof

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preparation example Construction

[0026] A preparation method of super heat-insulating aerogel foam concrete includes the following steps:

[0027] (1) Modification of aerogel powder;

[0028] (2) Dry mix the aerogel powder obtained in step (1) with the gelling material, and then add water to wet mix;

[0029] (3) Mix and stir the wet mixture obtained in step (2) with the prefabricated foam.

[0030] In addition, step (2) of the present invention can also be dry blending the gelling material, then adding water to wet blending, and adding the aerogel powder obtained in step (1) during wet blending.

[0031] In this way, the preparation method of the aerogel foam concrete of the present invention has the advantages of simple process, short process cycle, waste and environmental protection, etc., and is very suitable for industrial production.

[0032] In this embodiment, the step (1) includes a hydrophobic modification step; the hydrophobic modification step is to hydrophobically modify the aerogel powder in a closed hydro...

Embodiment 1

[0050] Use the following steps to prepare SiO 2 Aerogel foam concrete:

[0051] (1) Use a contact angle measuring instrument to detect the SiO to be processed 2 The contact angle between the surface of the aerogel powder and water, the test result is 55°, and the SiO with a particle size of 56μm 2 The aerogel powder is placed in a vacuum heating furnace, and the weighed hexamethyldisilazane is placed in a vacuum heating furnace with a container, heated and gasified, and hydrophobically modified for 1.5 hours to obtain hydrophobic SiO 2 Aerogel powder, use a contact angle measuring instrument to detect hydrophobic SiO 2 The contact angle between the surface of the aerogel powder and water is 147°;

[0052] (2) At room temperature, weigh ethanol, n-hexane, and deionized water at a mass ratio of 1:1:100, mix them evenly, and prepare a surface hydrophilic modification solution;

[0053] (3) Press hydrophobic SiO 2 The volume ratio of the aerogel powder and the surface hydrophilic modifica...

Embodiment 2

[0062] Use the following steps to prepare SiO 2 Aerogel foam concrete:

[0063] (1) Use a contact angle measuring instrument to detect the SiO to be processed 2 The contact angle between the surface of the aerogel powder and water, the test result is 45°, and the SiO with a particle size of 0.1mm 2 The aerogel powder is placed in a vacuum heating furnace, and the weighed trimethylchlorosilane is placed in a vacuum heating furnace with a container, heated and gasified, and hydrophobically modified for 1.5 hours to obtain hydrophobic SiO 2 Aerogel powder, use a contact angle measuring instrument to detect hydrophobic SiO 2 The contact angle between the surface of the aerogel powder and water is 146°;

[0064] (2) At room temperature, weigh the fatty alcohol polyoxyethylene ether ammonium sulfate, n-hexane, acetone and deionized water at a mass ratio of 1:0.4:0.4:130, mix them evenly, and configure the surface hydrophilic modification solution;

[0065] (3) Press hydrophobic SiO 2 The vo...

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Abstract

The invention discloses super-thermal-insulation aerogel foamed concrete and a preparation method thereof. The super-thermal-insulation aerogel foamed concrete is characterized by being prepared from aerogel powder and foamed concrete, wherein the aerogel powder comprises an inner hydrophobic layer and a surface hydrophilic layer, and the thickness of the surface hydrophilic layer is 0.1-100 mu m. The preparation method of the super-thermal-insulation aerogel foamed concrete comprises steps as follows: (1), the aerogel powder is modified; (2), the aerogel powder modified in the step (1) is subjected to dry blending with a cementitious material, and water is added to a mixture for wet blending; (3), a wet mixture obtained in the step (2) is mixed with prefabricated foam for stirring. The aerogel foamed concrete can be widely applied to the fields of thermal insulation, fire protection and sound insulation of walls, fire protection of steel structures and the like.

Description

Technical field [0001] The invention relates to a preparation method of a building insulation material, in particular to a super heat-insulating aerogel foam concrete and a preparation method thereof, belonging to the fields of lightweight, heat-insulating, fire-proof, sound-insulating materials and the like. Background technique [0002] With the progress of society, problems such as energy crisis and environmental degradation have become increasingly serious. In 2006, the "Outline of the Eleventh Five-Year Plan for National Economic and Social Development" put forward the concept of "energy saving and emission reduction" for the first time, and proposed a reduction in energy consumption per unit of GDP during the "Eleventh Five-Year Plan" period (2006-2010). It is a binding indicator of 10% reduction in the total discharge of major pollutants. "Energy saving" promotes "emission reduction". Building energy consumption accounts for 33% of the total domestic production energy con...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/04C04B28/06C04B38/02C04B38/10C04B14/06C04B20/02
CPCC04B20/023C04B28/04C04B28/065C04B2201/20C04B2201/32C04B2201/50C04B14/064C04B20/002C04B2103/0057C04B24/383C04B2103/302C04B22/147C04B24/14C04B38/106C04B22/085C04B24/38C04B22/148C04B24/16
Inventor 卢锋
Owner NANJING WEICAI NEW ENERGY TECH