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A low-temperature curing environmentally friendly water-based flocking adhesive

An adhesive and flocking technology, applied in the directions of cyclodextrin adhesives, adhesive types, chitin adhesives, etc. High strength, good weather resistance and good crack resistance

Active Publication Date: 2019-08-30
深圳市美之电实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a low-temperature-curing environmental-friendly water-based flocking adhesive, which uses natural and environmentally-friendly glutinous rice glue as the main component, has the advantages of high environmental protection, low-temperature curing, and good weather resistance, and solves the problem of low adhesion of ordinary glutinous rice glue. Poor antibacterial performance and prone to cracking

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1) 100g of montmorillonite, 20g of ammonium lauryl sulfate or sodium cetyl isethionate and 1200g of deionized water were stirred and reacted at 75°C for 3 hours, then filtered at room temperature, and the filter cake was dried, Grind and pass through a 60-mesh sieve to obtain 112 g of organically modified montmorillonite.

[0028] (2) Mix 100g of glutinous rice flour, 40g of potato starch and 110g of water evenly, gelatinize at 100°C for 15 minutes, then add 20g of compound enzyme, enzymolyze at pH 5.5, 75°C for 4 hours, After inactivating the enzyme for 10 minutes, lower the temperature to 55°C, then add 10g of organically modified montmorillonite, continue to stir and mix for 20-50 minutes, then add 10g of chitosan, continue to keep warm and stir, and then add 5g of β-cyclopaste after 10 minutes Refined to obtain 145g modified glutinous rice glue.

[0029] (3) A low-temperature curing environmentally friendly water-based flocking adhesive, consisting of the followin...

Embodiment 2

[0032] (1) 100g montmorillonite, 10g lauryl ammonium sulfate and 1500g deionized water were stirred and reacted at 70°C for 2.5 hours, then filtered at room temperature, the filter cake was dried and ground, and 101g organic modified Sexual montmorillonite.

[0033] (2) Mix 100g of glutinous rice flour, 30g of potato starch and 100g of water evenly, gelatinize at 90°C for 20 minutes, then add 10g of compound enzyme, enzymolyze at pH 5.5, 70°C for 5 hours, After inactivating the enzyme for 10 minutes, lower the temperature to 50°C, then add 20g of organically modified montmorillonite, continue stirring and mixing for 30 minutes, then add 10g of chitosan, continue to insulate and stir, and then add 5g of β-cyclodextrin after 10 minutes to obtain 132g modified glutinous rice glue; The compound enzyme is 3.5g cellulase, 6.5g α-amylase and 0.3g protease.

[0034] (3) A low-temperature curing environmentally friendly water-based flocking adhesive, consisting of the following compon...

Embodiment 3

[0037] (1) 100g montmorillonite, 30g sodium hexadecylsulfonate and 1000g deionized water were stirred and reacted at 80°C for 2 hours, then filtered at room temperature, the filter cake was dried and ground, and 122g organic modified montmorillonite.

[0038] (2) After mixing 100g of glutinous rice flour, 50g of potato starch and 120g of water evenly, gelatinize at 95°C for 10 minutes, then add 30g of compound enzyme, enzymolyze at pH 5.5, 80°C for 3 hours, and heat at 100°C After inactivating the enzyme for 10 minutes, lower the temperature to 60°C, then add 30g of organically modified montmorillonite, continue stirring and mixing for 50 minutes, then add 10g of chitosan, continue to insulate and stir, and then add 5g of β-cyclodextrin after 10 minutes to obtain 158g modified glutinous rice glue; The compound enzyme is 10g cellulase, 18g α-amylase and 2g protease.

[0039] (3) A low-temperature curing environment-friendly water-based flocking adhesive, consisting of the foll...

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Abstract

The invention provides a low-temperature setting environment-friendly water-based flocking adhesive which consists of the following components in parts by weight: 30 to 40 parts of modified glutinous rice glue, 5 to 8 parts of citric acid, 3 to 5 parts of thickener, 1 to 3 parts of emulsifier, 1 to 3 parts of antifoaming agent, 3 to 5 parts of preservative, 2 to 4 parts of D-glucose, 3 to 5 parts of silane coupling agent and 8 to 10 parts of deionized water. A preparation method of the improved glutinous rice glue comprises: after uniformly mixing glutinous rice flour, potato starch and water, carrying out high-temperature gelatinization, compound enzyme enzymolysis and enzyme denaturing; cooling to a temperature of 50 to 60 DEG C; then sequentially adding organic improved montmorillonite, chitosan and beta-cyclodextrin. The flocking adhesive provided by the invention uses the natural environment-friendly glutinous rice glue as a main ingredient, has the advantages of high environment-friendliness, low-temperature setting and good weather resistance and meanwhile, solves the problems of low cohesiveness, poor antibacterial property and easiness for generating cracks of common glutinous rice glue.

Description

technical field [0001] The invention belongs to the technical field of adhesives, and in particular relates to a flocking adhesive, in particular to a low-temperature curing environment-friendly water-based flocking adhesive. Background technique [0002] Electrostatic flocking is prepared by planting electro-treated short fibers on the surface of the substrate coated with adhesive in a high-voltage electrostatic field, and then pre-baking, baking and other processes. As a surface processing technology, electrostatic flocking has its unique advantages. It can be flocked on various three-dimensional and non-three-dimensional substrates such as fabric, paper, plastic, rubber, wood, glass, metal and ceramics. It has been widely used in Automobiles, stationery, packaging, decoration, instruments and meters and many other industries, and have the functions of wear resistance, lubrication, sealing, sound insulation, heat insulation, anti-scalding, anti-corrosion and anti-fouling, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J103/12C09J105/08C09J105/16C09J11/08C09J11/06C09J11/04
Inventor 陈林梭
Owner 深圳市美之电实业有限公司
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