Preparation method and application of aspartic acid Maillard reactant

A technology of aspartic acid Maillard and Maillard reaction, which is applied in the fields of application, preparation of tobacco, food science, etc., can solve the problems of difficult to widely use cigarettes, lack of coloring ability, and single flavor of spices, etc., to improve the appearance and sensory quality, appearance and sensory quality improvement, simple and mild process conditions

Active Publication Date: 2020-11-03
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The source of raw materials of this method is complicated, the cost is high, and the flavor type of the prepared spice is relatively single, so it is difficult to be widely used in cigarettes.
Other maillard reaction spices with complex sugar sources and nitrogen sources have complex sources of raw materials and high costs. The prepared Maillard reaction products are complex and difficult to purify, causing greater irritation to smoke
Authorized invention patent ZL201310268308.X "A method for preparing tobacco flavor by regulating the Maillard reaction", the amino acid and glucose are mixed and dissolved in water according to the mass ratio of 1:2 to 1:6 to obtain the initial mixed liquid, and the initial mixed The mass concentration of glucose in the solution is 10% to 20%, the pH is 8 to 12, and the temperature is controlled at 105°C to 120°C for 0.5 to 1 hour; add L-ascorbic acid and continue to react at 105°C to 120°C for 0.5 to 1 hour to prepare Demaillard reaction type tobacco flavor, the Maillard reaction flavor has the defects of high polysaccharide content, complex components, high viscosity, strong moisture absorption, and almost no coloring ability
The existing reports of the Maillard reaction product of aspartic acid are propylene glycol / water system, the ratio of aspartic acid and reducing sugar is usually 1:2~1:1.2, the sugar is excessive, and the catalyst is ammonia water and hydroxybutyl anise Ether or tert-butyl hydroquinone, etc., the reactants have the defects of many impurities, high polysaccharide content, and high moisture absorption. There is no aspartic acid Maillard reactant to improve the appearance and appearance of reconstituted tobacco leaves and their wrappers. sensory quality reports

Method used

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  • Preparation method and application of aspartic acid Maillard reactant
  • Preparation method and application of aspartic acid Maillard reactant
  • Preparation method and application of aspartic acid Maillard reactant

Examples

Experimental program
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Embodiment 1

[0029] A preparation method of aspartic acid Maillard reactant, specifically comprising the steps of:

[0030](1) Raw material preparation: aspartic acid and reducing sugar (rhamnose and caramel, the molar ratio is 1:2) are configured in a molar ratio of 2.8:1, and the catalyst is ammonium acetate and ascorbic acid (mass ratio 1:0.5), The total mass of the catalyst accounts for 0.5% of the total mass of the Maillard reaction substrate; the mass ratio of water to the Maillard reaction substrate is 2:1;

[0031] (2) Production and preparation: first add water to the reaction tank, start the stirring motor, heat to 50°C, add aspartic acid and reducing sugar in proportion in turn, stir thoroughly until they are completely dissolved, then add the catalyst; during the reaction , set the process condition of the Maillard reaction tank as temperature 125°C, keep the stirring motor on, and the reaction time is 6h;

[0032] (3) Finished product: After the reaction, the reactant is natu...

Embodiment 2

[0035] A preparation method of aspartic acid Maillard reactant, specifically comprising the steps of:

[0036] (1) Raw material preparation: amino acids (aspartic acid and asparagine in a molar ratio of 1:1) and fermented coconut extract are used as Maillard reaction substrates, and the mass ratio of amino acids to fermented coconut extract is 2.5:1 To configure; Catalyst is ascorbic acid, ammoniacal liquor, ammonium bicarbonate (configuration by equal mass ratio), and catalyst gross mass accounts for 1% of the Maillard reaction substrate gross mass; The mass ratio of water and Maillard reaction substrate is 2.5: 1;

[0037] (2) Production preparation: first add water into the reaction tank, start the stirring motor, heat to 55°C, add amino acid and fermented coconut extract in a certain proportion in turn, stir thoroughly until completely dissolved, then add the catalyst; during the reaction , set the process condition of the Maillard reaction tank as temperature 105°C, keep...

Embodiment 3

[0042] A preparation method of aspartic acid Maillard reactant, specifically comprising the steps of:

[0043] (1) Raw material preparation: Asparagine and sugar source (3:1 by mass ratio) are used as the substrate of the Maillard reaction, and the sugar source is a composite of mannose, rhamnose, xylose, and fermented coconut extract substance (mass ratio is 1:1:1:0.6); catalyst is ammonium acetate, ascorbic acid, decanal (equal mass ratio), and the total mass accounts for 1.2% of the Maillard reaction substrate mass; water and Maillard reaction bottom The mass ratio of the substance is 2.2:1;

[0044] (2) Production preparation: first add water into the reaction tank, start the stirring motor, heat to 60°C, add asparagine and sugar source in a certain proportion in turn, stir thoroughly until completely dissolved, then add the catalyst; during the reaction , set the process condition of the Maillard reaction tank to a temperature of 98°C, keep the stirring motor on, and the...

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Abstract

The invention aims at providing a preparation method of aspartic acid Maillard reactant and applications of the aspartic acid Maillard reactant in reconstituted tobacco and cigar wrappers. By adding a certain percentage of amino acid (aspartic acid or / and asparagine), reducing sugar and catalyst into a Maillard reaction tank and performing Maillard reaction under certain technological conditions to industrially produce aspartic acid hyperchromic and fragrance-strengthening Maillard reactant, impurities of polysaccharide and the like can be reduced, the defects of moisture absorption, irritating and the like can be reduced; after being applied to the reconstituted tobacco and cigar wrappers, the appearance and feeling quality of the reconstituted tobacco and cigar wrappers can be improved, smoke can be coordinated, and baking and scorched sweet fragrance can be increased, so that smoke is soft and fine, the irritating property of smoke can be reduced, the sensory quality can be improved, the appearance is close to the appearance color of cigars and is natural and uniform, and the technological conditions are mild and easy to operate, and the cost is low.

Description

technical field [0001] The invention relates to the technical field of tobacco additives, in particular to a preparation method of aspartic acid Maillard reactant and its application in reconstituted tobacco leaves and wrappers. Background technique [0002] With the improvement of people's health awareness, the difficulties faced by cigarette factories in solving the problem of reducing the amount of cigarette tar while maintaining or satisfying the availability of cigarette smoking have become increasingly prominent. As one of the important ways to form the characteristic aroma of tobacco, the Maillard reaction has been favored for its application in tobacco flavoring. The aroma produced by the reaction is also different according to the sugar source and nitrogen source, and a large amount of heterocyclic aroma compounds are produced by the reaction, which can improve the smoke of cigarettes. [0003] Reconstituted tobacco can be used as a raw material for tobacco product...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00A24B3/12
CPCA24B3/12C11B9/0003
Inventor 魏敏陈义坤宋旭艳潘曦罗诚浩李冉高颂刘志昌姚元军
Owner HUBEI CHINA TOBACCO IND
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