Adhesive for laminating metal foil and resin film, laminated body, packaging material for battery exterior, and battery case and method for manufacturing same
A resin film and metal foil technology is applied to a battery case and a manufacturing method of the battery case. . It can solve the problems of unstable operability, deviation of the adhesive force of the adhesive layer, poor adhesion, etc., and achieve the effect of good and excellent balance of heat resistance and electrolyte resistance, excellent adhesion, and long life.
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[0142] Hereinafter, although an Example and a comparative example demonstrate this invention more concretely, this invention is not limited by these Examples at all.
Synthetic example 1
[0144] Into a reaction vessel equipped with a stirrer and a water separator, 220.00 g of "Sovermol908" (manufactured by BASF Corporation) as a hydrogenated dimer glycol, 230.00 g of "EMPOL1008" (manufactured by BASF Corporation) as a hydrogenated dimer acid, and The catalyst was 0.10 g of butyltin dilaurate "KS-1260" (manufactured by Sakai Chemical Industry Co., Ltd.), and at about 240° C., the dehydration esterification reaction was carried out under reduced pressure while flowing out condensation water from normal pressure to obtain poly Ester polyol (hereinafter referred to as polyester polyol (1).).
Synthetic example 2
[0146] Into a reaction container equipped with a stirring device, a thermometer, and a condenser, 108.00 g of "GI-1000" (manufactured by Nippon Soda Co., Ltd., hydrogenated polybutadiene polyol) as the component (a11) and 108.00 g of the component (a2) were charged. 12.00 g of "TCD Alcol DM" (manufactured by Oaksea Co., Ltd., tricyclodecane dimethanol), 0.04 g of hydroquinone monomethyl ether (manufactured by Wako Pure Chemical Industries, Ltd.) as an antioxidant, and "KS- 1260" (manufactured by Sakai Chemical Industry Co., Ltd., dibutyltin dilaurate) 0.03 g, "Desmogel W" (manufactured by Baiel Co., Ltd., methylene bis(4-cyclohexyl isocyanate)) as the component (a3) 30.00 g and While stirring 70.00 g of toluene as a solvent (D), the temperature was raised to 85 to 90° C. using an oil bath. Then, the reaction was continued while stirring for 2.5 hours. Then, measure the infrared absorption spectrum, confirm that the absorption of isocyanate group disappears, finish reaction,...
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Abstract
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