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Plasma anodic nitriding surface strengthening process for duplex stainless steel

A duplex stainless steel, plasma technology, applied in metal material coating process, solid diffusion coating, coating and other directions, can solve the problems of reducing the working efficiency of equipment, inability to achieve three-phase separation, and easy blockage of the feeding system, etc. Achieve the effect of avoiding roughening damage, high hardness and short cycle

Active Publication Date: 2020-02-18
NANJING INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the drum assembly of the disc starch separator manufactured in my country is composed of multiple parts, and the internal structure is complicated. Not only is the assembly cumbersome, but also the feeding system is easy to block. The equipment must be stopped to clean the drum after ten days of operation, and three-phase separation cannot be achieved. , which greatly reduces the working efficiency of the equipment
Western developed countries have done early research in the field of solid-liquid separation, and the current technology is relatively comprehensive and complete, and there are a large number of commercial application examples, but the products of these companies are extremely expensive, and equipment maintenance is troublesome and relatively expensive.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A duplex stainless steel plasma anodic nitriding surface strengthening process, the technical scheme of which comprises the following steps:

[0020] (1) Duplex stainless steel surface pretreatment: the main process includes: degrease the duplex stainless steel with trichlorethylene solvent, then dip and clean it with industrial detergent at 90°C for 10 minutes, and then wash it with water at 93°C drying under the sun to obtain the duplex stainless steel after surface pretreatment;

[0021] (2) Plasma-assisted anode nitriding: use plasma-assisted anode nitriding technology to carry out surface modification and strengthening treatment on the ultra-low carbon duplex stainless steel disc, and the duplex stainless steel after the surface pretreatment described in step (1) Put it into the anode nitriding device, control the nitriding process parameters, the partial pressure of argon gas is 0.5Pa, the partial pressure of nitrogen gas is 500Pa, the bias voltage is 800V, the ni...

Embodiment 2

[0024] A duplex stainless steel plasma anodic nitriding surface strengthening process, the technical scheme of which comprises the following steps:

[0025] (1) Duplex stainless steel surface pretreatment: the main process includes: degrease the duplex stainless steel with ethyl hexanoate solvent, then dip and clean it with industrial detergent at 83°C for 15 minutes, then wash it with water, and then wash it at 70 Dry at ℃ to obtain the duplex stainless steel after surface pretreatment;

[0026] (2) Plasma-assisted anode nitriding: use plasma-assisted anode nitriding technology to carry out surface modification and strengthening treatment on the ultra-low carbon duplex stainless steel disc, and the duplex stainless steel after the surface pretreatment described in step (1) Put it into the anode nitriding device, control the nitriding process parameters, the partial pressure of argon gas is 0.05Pa, the partial pressure of ammonia gas is 150Pa, the bias voltage is 200V, the nit...

Embodiment 3

[0029] A duplex stainless steel plasma anodic nitriding surface strengthening process, the technical scheme of which comprises the following steps:

[0030] (1) Duplex stainless steel surface pretreatment: the main process includes: degrease the duplex stainless steel with acetone solvent, then dip and clean it with industrial detergent at 70°C for 15 minutes, then wash it with water, and dry it at 93°C , the obtained duplex stainless steel after surface pretreatment;

[0031] (2) Plasma-assisted anode nitriding: use plasma-assisted anode nitriding technology to carry out surface modification and strengthening treatment on the ultra-low carbon duplex stainless steel disc, and the duplex stainless steel after the surface pretreatment described in step (1) Put it into the anode nitriding device, control the nitriding process parameters, the partial pressure of argon gas is 0.3Pa, the partial pressure of nitrogen gas and ammonia gas (volume ratio is 2:1) is 0.5Pa, the bias voltag...

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Abstract

The invention discloses a duplex stainless steel plasma anode nitriding surface strengthening technology. The duplex stainless steel plasma anode nitriding surface strengthening technology comprises the following steps that (1) duplex stainless steel surface pretreatment is carried out; (2) plasma auxiliary anode nitriding is carried out, wherein a plasma auxiliary anode nitriding technology is adopted for conducting surface modification and strengthening processing on ultra-low carbon duplex stainless steel discs, and duplex stainless steel obtained after surface pretreatment is placed into an anode nitriding device for nitriding treatment; and (3) annealing is carried out. By means of the duplex stainless steel plasma anode nitriding surface strengthening technology, formation of a brittle phase can be effectively restrained, the discs have the excellent toughness matching from the surface layers to the center parts, workpiece secondary deformation caused by temperature gradient is reduced as many as possible on the basis of guaranteeing the excellent texture uniformity and mechanical property, coarsening damage caused by arc striking, edge effects and the like on treated surfaces can be avoided, meanwhile, formation of the white and bright semi-stable state compound S phase is better achieved, separation of brittle phases such as epsilon-Fe2-3N and gamma'-Fe4N is restrained,and the discs have the higher hardness, abrasion resistance and erosion resistance.

Description

technical field [0001] The invention relates to a metal surface strengthening technology, in particular to a dual-phase stainless steel plasma anode nitriding surface strengthening technology, which uses plasma-assisted anode nitriding technology to perform surface modification and strengthening treatment on ultra-low carbon duplex stainless steel discs . Background technique [0002] At present, the domestic starch separator is a nozzle continuous discharge type disc separator, which is mainly used for starch refining, pre-concentration, protein separation and starch recovery in the starch industry, and can also be used in food, medicine, dyeing, environmental protection and other departments. Processes such as liquid-solid two-phase separation, concentration recovery and clarification, such as kaolin, pulp recovery, wastewater treatment, etc. The manufacturing time of disc starch separator in our country is relatively short, and its main technology has been digested and a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C8/38C23C8/26C23C8/02C21D1/26C23F17/00
CPCC21D1/26C23C8/02C23C8/26C23C8/38C23F17/00
Inventor 王章忠牟富君张保森王斌张端涛李力成张震卫杭志锋
Owner NANJING INST OF TECH
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