The invention belongs to the technical field of
metal materials and
powder metallurgy, and discloses a preparation method of a TiB2 enhanced AlCoCrFeNi high-entropy
alloy, which comprises the following steps: S1, weighing raw materials: weighing Al, Co, Cr, Fe and Ni
metal powder according to an equal
atomic ratio, and weighing TiB2
powder which accounts for 5-20% of the total
mass of the Al, Co, Cr, Fe and Ni
metal powder; s2, mechanical alloying
machining is conducted, specifically, Al, Co, Cr, Fe and Ni
metal powder and TiB2 powder are mixed and then subjected to high-energy ball milling
machining, and composite powder is obtained; s3, molding
processing:
drying and sieving the composite powder in the S2, and loading the composite powder into a mold for cold press molding to obtain a
green body; and S4,
atmosphere protection
sintering is conducted, specifically, the
green body is placed in
sintering equipment under
inert atmosphere protection to be sintered, and the TiB2 reinforced AlCoCrFeNi high-entropy
alloy is obtained. According to the preparation method, high-dispersion distribution of TiB2 particles in
alloy powder is achieved through high-energy ball milling, and a bulk material which is uniform in structure and high in density is obtained in cooperation with a
sintering process.