Magnetic carboxylation hollow microsphere soil restoration agent as well as preparation method and application thereof
A technology of soil remediation agent and hollow microspheres, which is applied in the direction of chemical instruments and methods, restoration and application of contaminated soil, etc., can solve problems such as weak salt-alkali resistance, long repair time, and low specificity, and achieve Shorten the curing time, reduce the amount of dosage, and have strong specificity
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Embodiment 1
[0049] A preparation method of magnetic carboxylated hollow microsphere soil repair agent, comprising the following steps:
[0050] Step 1, using the improved monodisperse SiO 2 Microspheres
[0051] Step 1.1, mix 6ml of concentrated ammonia water, 49.5ml of absolute ethanol and 18ml of deionized water, then magnetically stir at 35°C for 20min, and obtain solution A after stirring;
[0052] Step 1.2, mix 3ml tetraethyl orthosilicate with 49.5ml absolute ethanol, then magnetically stir at 35°C for 20min, and obtain solution B after stirring;
[0053] Step 1.3, quickly pour solution B into solution A, and then react at 35°C. After 35 minutes of reaction, a milky white precipitate begins to appear. Continue to react for 5 minutes, and the milky white precipitate is separated to obtain monodisperse SiO 2 Microspheres;
[0054] Step 2, hydrothermal synthesis of Fe 3 o 4 @C hollow microsphere
[0055] Step 2.1, 0.0506g of SiO prepared in step 1 2 Put in a beaker, pour 60ml ...
Embodiment 2
[0067] Taking the farmland soil near the metal smelter polluted by heavy metal lead as the soil sample, adjust the organic matter content in the lead-contaminated soil to be restored to 63.04g kg -1 , pH is 7.33, conductivity is 142.60μs·cm -1 , The moisture content is 50%.
[0068] It should be noted that when adjusting the content of organic matter in the soil to be restored, when the content of organic matter in the polluted soil is detected to be too low, organic matter such as dry animal manure with a particle size of 1-2 mm or composted crop straw and other organic matter can be added to increase the soil organic matter; When the content of soil organic matter is too high, spray a certain concentration of potassium permanganate solution on the polluted soil to oxidize and decompose the soil organic matter; the organic matter plays an auxiliary role in the curing process, mainly promoting the adsorption and complexation of heavy metals by the restoration agent.
[0069] ...
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