A temperature-resistant diaphragm for solar lithium battery and solar lithium battery
A lithium battery and solar energy technology, applied in lithium batteries, battery pack components, non-aqueous electrolyte batteries, etc., can solve the problems of aggravated heat accumulation, high risk, easy to melt, etc., to achieve good charging and discharging efficiency, good resistance Corrosive, low thermal shrinkage effect
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Embodiment 1
[0026] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0027] Wherein, the preparation method of described cellulose film comprises the steps:
[0028] A, adding 3 parts by weight of nanocellulose to 25 parts by weight of an aqueous ethanol solution with a volume concentration of 95% for ultrasonic dispersion to obtain a dispersion;
[0029] B. Add 33 parts by weight of ethyl orthosilicate to the dispersion, adjust the pH to 9.5 with ammonia water to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0030] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0031] D. At a temperature of 80°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mas...
Embodiment 2
[0041] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0042] Wherein, the preparation method of described cellulose film comprises the steps:
[0043]A, adding 1 weight part of nanocellulose to 20 weight parts of ethanol aqueous solution with a volume concentration of 92% for ultrasonic dispersion to obtain a dispersion;
[0044] B. Add 28 parts by weight of ethyl orthosilicate to the dispersion, use ammonia water to adjust the pH to 9 to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0045] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0046] D. At a temperature of 70°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mass ratio of ...
Embodiment 3
[0056] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0057] Wherein, the preparation method of described cellulose film comprises the steps:
[0058] A, adding 5 parts by weight of nanocellulose to 30 parts by weight of an aqueous ethanol solution with a volume concentration of 98% for ultrasonic dispersion to obtain a dispersion;
[0059] B. Add 38 parts by weight of ethyl orthosilicate to the dispersion, use ammonia to adjust the pH to 10 to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0060] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0061] D. At a temperature of 90°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mass rat...
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