Preparation method and application of a hot pot food matrix papaverine standard substance
A standard substance, papaverine technology, applied in the preparation of hot pot food matrix papaverine standard substance, in the field of matrix standard substance, it can solve problems such as difficult to meet, expensive price, unsatisfactory monitoring, etc.
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Embodiment 1
[0021] 1 Materials and methods
[0022] 1.1 Instruments, utensils and reagents
[0023] 1.1.1 Instrument: API3500 liquid mass spectrometer, distribution electrospray ion source (ESI source), positive ion monitoring mode: Urel = 5%, k = 2; electronic balance: Class I, resolution 0.0001g, maximum allowable The error is ±0.05mg; the expanded uncertainty of the weighing balance is U=0.6mg (k=2).
[0024] 1.1.2 Vessels: 100mL volumetric flask: Grade A, with a maximum allowable error of ±0.10mL; 10mL volumetric flask (Grade A), with a maximum allowable error of ±0.015mL at 20°C; 1mL pipette (apparatus number JS2012002): Grade A , the maximum allowable error is ±1.0%; 10mL graduated pipette: Grade A, the maximum allowable error is ±0.05mL; 2mL graduated pipette: A grade, the maximum allowable error is ±0.012mL.
[0025] 1.1.3 Main reagents: papaverine standard substance: purity ≥ 98.00% ± 0.5%, Stanford Analytical Chemicals Inc, USA; chromatography grade reagents for acetonitrile a...
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