High temperature resistant adhesive and its preparation method and composite insulating paper
A composite insulation and adhesive technology, applied in the direction of adhesives, adhesive additives, polymer adhesive additives, etc., can solve the problems of large energy consumption and large pollution
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[0021] The present invention also provides a method for preparing a high-temperature-resistant adhesive, which includes: adding each component of the above-mentioned high-temperature-resistant adhesive into a mixer, and stirring evenly.
[0022] In the method for preparing the high temperature resistant adhesive of the present invention, preferably, the stirring temperature is 70-110°C.
[0023] The present invention also provides a composite insulating paper, the composite insulating paper sequentially includes: a first fiber paper, a polyimide film, a second fiber paper; between the first fiber paper and the polyimide film, the The above-mentioned second fiber paper and the polyimide film are bonded by the high temperature resistant adhesive provided by the present invention.
[0024] In the composite insulating paper of the present invention, preferably, the first fiber paper is one or more of polyaramid fiber paper, polysulfone amide fiber paper, and inorganic fiber paper;...
Embodiment 1
[0031] Based on the total weight of the high-temperature resistant adhesive, 70% by weight of cyanate resin and 3% by weight of polysiloxane-modified cyanate resin were stirred at 90°C; Hydroxyl hyperbranched polysiloxane, 6% by weight of nonylphenol, stirred and mixed evenly at 90° C. to obtain adhesive P1;
[0032] The above adhesive was cooled to 70°C and then coated on both sides of the polyimide film, and then combined with polyaramid fiber paper (Nomex 464 from DuPont Company) and cured at 110°C for 10 hours to obtain composite insulating paper PS1.
Embodiment 2
[0034] Based on the total weight of the high temperature resistant adhesive, 60% by weight of cyanate resin and 5% by weight of polysiloxane modified cyanate resin were stirred at 70°C; Epoxy hyperbranched polysiloxane, 8% by weight of nonylphenol, stirred and mixed evenly at 70°C to obtain adhesive P2;
[0035] The above adhesive was cooled to 50°C and coated on both sides of the polyimide film, and then combined with inorganic fiber paper (TufQUIN110 from 3M Company) and cured at 120°C for 10 hours to obtain composite insulating paper PS2.
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