Preparation method of bearing steel large sample electrolytic sample
A technology for bearing steel and large samples, applied in the field of test sample preparation, can solve problems such as affecting the accuracy of experimental results, flaky metal shedding, and increasing working strength, so as to prevent lamellar metal shedding on the surface of the sample , Improve accuracy and reduce labor intensity
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[0012] The preparation method of the bearing steel large-scale electrolytic sample of the present invention adopts the following process: (1) Sampling: On the rolled material, cut a cuboid rough sample of 65 ± 5 mm × 65 ± 5 mm × (180-200) mm, or a diameter Cylindrical rough sample with a diameter of 65±5mm and a length of 180-200mm.
[0013] (2) Spheroidizing annealing: heat the crude sample with the heating furnace, heat it to 790-810°C, and keep it warm for 3-6 hours; then cool it with the furnace (with the furnace door closed), and the cooling rate is preferably 20-60°C / h; After the furnace temperature drops to 650°C or below, take it out and air cool it.
[0014] (3) Post-treatment: Car polish or polish the surface of the coarse sample after spheroidizing annealing until the surface finish is at least ▽6; then degrease with a degreasing agent (ethanol, acetone or carbon tetrachloride), and then use a volumetric Wash the surface with a dilute HCl solution with a ratio of 1...
Embodiment 1
[0015] Embodiment 1: The method for preparing a large electrolytic sample of bearing steel according to the present invention is specifically described as follows.
[0016] (1) On the GCr15 rolled material, cut two cylindrical rough samples with a diameter of 65mm and a length of 190mm at the same position along the rolling direction, and mark them as 1 and 2 respectively.
[0017] (2) Spheroidizing annealing treatment: Put the crude sample 2 into the heating furnace, heat it up to 800°C with the furnace, and then start to keep it warm, keep it at 800°C for 4 hours, and cool it with the furnace (furnace door closed), the cooling rate is 40~60℃ / h, when the furnace temperature drops to 650℃, take it out and air cool.
[0018] (3) The surface of rough sample 2 after spheroidizing annealing and rough sample 1 without annealing was polished to a surface roughness of ▽8, then degreased with a degreasing agent, and then dilute HCl solution with a volume ratio of 1:4 Clean the surfac...
Embodiment 2
[0022] Embodiment 2: The preparation method of the bearing steel large sample electrolysis sample of the present invention is specifically described as follows.
[0023] (1) On the GCr18Mo rolled material, cut two 70mm×65mm×180mm cuboid rough samples at the same position along the rolling direction, and mark them as 1 and 2 respectively.
[0024] (2) Spheroidizing annealing treatment: Put the crude sample 2 into the heating furnace, heat it up to 810°C with the furnace, then start to keep it warm, keep it at 810°C for 6 hours, and cool it with the furnace (furnace door closed), the cooling rate is 20~40°C / h, when the furnace temperature drops to 630°C, take it out and cool it in air.
[0025] (3) The rough sample 2 after spheroidizing annealing and the rough sample 1 without annealing were polished to a surface roughness of ▽6, then degreased with a degreasing agent, and then dilute HCl solution with a volume ratio of 1:5 Clean the surface to make a large cuboid electrolytic ...
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