Eureka AIR delivers breakthrough ideas for toughest innovation challenges, trusted by R&D personnel around the world.

Method for producing temperature measuring tungsten-rhenium thermocouple wires in high-reliability manner through combined technology

A technology of thermocouple wire and reliability, which is applied in the field of powder metallurgy manufacturing, can solve the problems of large difference in thermoelectric potential between the head and the tail of the couple wire, difficult to press and sinter, and cannot be completely replaced, so as to improve the level of process control, uniform composition, and improve consistent effect

Active Publication Date: 2019-07-19
无锡国涛钨铼合金科技有限公司
View PDF8 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology describes methods used during production of wires made from tantalum ruthenium (Ta) alloys. These techniques aimed towards producing pure metallic Ta particles while maintaining their quality. By selecting specific elements based on these properties, it was possible to achieve better results than previous methods without compromising its performance. Additionally, this technique allows for easier handling and processing of raw material compared to current processes such as solid state reactions. Overall, this new approach resulted in higher efficiency and precision in thermal measurements over time.

Problems solved by technology

The technical problem addressed by this patented technology relates to producing pure metallurgically strong materials with good properties such as resisting corrosion or abrasion while maintaining their heat transfer capabilities at temperatures above 1000°C (hot). This can lead to improved performance characteristics over time when exposed to these extreme environments.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for producing temperature measuring tungsten-rhenium thermocouple wires in high-reliability manner through combined technology
  • Method for producing temperature measuring tungsten-rhenium thermocouple wires in high-reliability manner through combined technology
  • Method for producing temperature measuring tungsten-rhenium thermocouple wires in high-reliability manner through combined technology

Examples

Experimental program
Comparison scheme
Effect test

Embodiment l

[0024] A method for producing tungsten-rhenium thermocouple wire for temperature measurement with high reliability by using combined technology

[0025] This embodiment takes WRe5.45 tungsten-rhenium thermocouple wire as an example to illustrate

[0026] (1) Preparation method:

[0027] 1) Preparation of tungsten-rhenium alloy compound powder by full liquid phase mixing method: 1 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water, and 0.058 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water. Dissolve ammonium rhenate in water, stir ammonium tungstate aqueous solution and ammonium perrhenate aqueous solution at 85°C, and then use spray crystallization method to make such figure 1 Tungsten-rhenium alloy compound powder shown.

[0028] 2) Tablet preparation to obtain debris: place the tungsten-rhenium alloy compound powder obtained in step 1) at a unit pressure of 60kg / cm 2 The st...

Embodiment 2

[0041]A method for producing tungsten-rhenium thermocouple wire for temperature measurement with high reliability by using combined technology

[0042] This embodiment takes WRe5.45 tungsten-rhenium thermocouple wire as an example for illustration

[0043] (1) Preparation method:

[0044] 1) Preparation of tungsten-rhenium alloy compound powder by full liquid phase mixing method: 1 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water, and 0.058 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water. Dissolve ammonium rhenate in water, stir ammonium tungstate aqueous solution and ammonium perrhenate aqueous solution at 95°C, and use spray crystallization method to make such figure 1 Tungsten-rhenium alloy compound powder shown.

[0045] 2) Tablet preparation to obtain debris: place the tungsten-rhenium alloy compound powder obtained in step 1) at a unit pressure of 150kg / cm 2 The stan...

Embodiment 3

[0058] A method for producing tungsten-rhenium thermocouple wire for temperature measurement with high reliability by using combined technology

[0059] This embodiment takes WRe5.45 tungsten-rhenium thermocouple wire as an example for illustration

[0060] (1) Preparation method:

[0061] One) preparation method:

[0062] 1) Preparation of tungsten-rhenium alloy compound powder by full liquid phase mixing method: 1 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water, and 0.058 kg of commercially available ammonium tungstate with a purity of 4N (99.99%) was dissolved in water. Dissolve ammonium rhenate in water, stir ammonium tungstate aqueous solution and ammonium perrhenate aqueous solution at 100°C, and then use spray crystallization method to make such figure 1 Tungsten-rhenium alloy compound powder shown.

[0063] 2) Tablet preparation to obtain debris: place the tungsten-rhenium alloy compound powder obtained in step 1) ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Wire diameteraaaaaaaaaa
Diameteraaaaaaaaaa
Login to View More

Abstract

The invention relates to a method for producing temperature measuring tungsten-rhenium thermocouple wires in high-reliability manner through a combined technology. Through the technical scheme, ammonium tungstate with purity 4N and ammonium perrhenate with purity 4N are made into a solution, through spray crystallization, tungsten-rhenium alloy compund powder is made, the powder is pressed into broken pieces and then is subjected to hydrogen reduction, then, the pieces are pressed and sintered into metal bars, and through rotary swaging, annealing and wire drawing, the needed diameter is obtained; the problems that the full-liquid-phase mixed powder grains are too fine, bar making is difficult, after process penetrating, components of all segments of the head, the middle and the tail of the wire strip are not consistent, thermoelectric potential difference is too large, and the subsequent pairing is not accurate are solved. Through the method, making convenience degree of the temperature measuring tungsten-rhenium thermocouple wires and the temperature measuring precision of the temperature measuring tungsten-rhenium thermocouple wires are obviously improved, and the method has thegiant scientific significance and application value in improving the process control level, and reducing the control material part unit cost in many industries, particularly, the high-technology manufacturing industry, in the national economy.

Description

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Owner 无锡国涛钨铼合金科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Eureka Blog
Learn More
PatSnap group products