A kind of high adhesion PE protective film and preparation method thereof
A technology of adhesion and protective film, applied in the direction of polymer adhesive additives, non-polymer adhesive additives, adhesives, etc., can solve the problem of easy peeling off of the PE film layer, and achieve high bonding fastness and enhanced adhesion. The effect of compatibility and improving compatibility
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Embodiment 1
[0054] A kind of tea saponin-acrylate base wetting agent, adopts following method to prepare:
[0055] (1) Add 15 parts of acrylic acid, 20 parts of methyl acrylate, 10 parts of double bond-containing silicone, 50 parts of water, and 0.5 parts of carboxylic acid type compatibilizer into a three-necked flask for stirring, the stirring speed is 130~140r / min, And feed nitrogen flow, heat up to 55°C under nitrogen environment, keep warm for 20min;
[0056] (2) Add 1 part of polyoxyethylene hydrogenated castor oil and 1 part of sodium lauryl sulfate to step (1), stir evenly, and heat up to 75°C;
[0057] (3) Add 0.1 parts of benzoyl to step (2), keep stirring, and react for 1.5~2h;
[0058] (4) Add 20 parts of tea saponin and soak for 2 hours.
Embodiment 2
[0060] A kind of tea saponin-acrylate base wetting agent, adopts following method to prepare:
[0061] (1) Add 18 parts of acrylic acid, 22 parts of methyl acrylate, 12 parts of double bond-containing silicone, 52 parts of water, and 1 part of carboxylic acid compatibilizer into a three-necked flask and stir at a stirring speed of 130~140r / min. And feed nitrogen flow, heat up to 55°C under nitrogen environment, keep warm for 20min;
[0062] (2) Add 1~3 parts of polyoxyethylene hydrogenated castor oil and 1~2 parts of sodium lauryl sulfate to step (1), stir evenly, and heat up to 75°C;
[0063] (3) Add 0.1~0.3 parts of benzoyl to step (2), keep stirring, and react for 1.5~2h;
[0064] (4) Add 25 parts of tea saponin and soak for 2 hours.
Embodiment 3
[0066] A kind of tea saponin-acrylate base wetting agent, adopts following method to prepare:
[0067] (1) Add 18 parts of acrylic acid, 23 parts of methyl acrylate, 13 parts of double bond-containing silicone, 52 parts of water, and 1 part of carboxylic acid compatibilizer to a three-necked flask and stir at a stirring speed of 130~140r / min. And feed nitrogen flow, heat up to 55°C under nitrogen environment, keep warm for 20min;
[0068] (2) Add 1.5 parts of polyoxyethylene hydrogenated castor oil and 1.5 parts of sodium lauryl sulfate to step (1), stir evenly, and heat up to 75°C;
[0069] (3) Add 0.2 parts of benzoyl to step (2), keep stirring, and react for 1.5~2h;
[0070] (4) Add 30 parts of tea saponin and soak for 2 hours.
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Abstract
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