Low-carbon magnesium-carbon refractory material added with silicon magnesium nitride powder and preparation method thereof
A technology of carbon-magnesium-carbon refractories and silicon-magnesium nitride, which is applied in the field of low-carbon magnesium-carbon refractories, can solve the problems of unfavorable industrial production, increased production costs, and high addition of antioxidants.
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Embodiment 1
[0048] A low-carbon magnesium-carbon refractory material added with magnesium silicon nitride powder and a preparation method thereof. The steps of the preparation method described in this embodiment are:
[0049] Step 1. Use 40-43wt% fused magnesia particles, 42-45wt% fused magnesia fine powder, 7-8wt% flake graphite, 5.5-6wt% phenolic resin and 2-3wt% nitriding Magnesium silicon powder is used as raw material and ingredients.
[0050] Step 2. Add the magnesium silicon nitride powder into the phenolic resin in 3 to 5 times at 40 to 50° C. and under magnetic stirring conditions, and stir for 15 to 20 minutes each time to obtain a mixture, which is taken out for use.
[0051] Step 3. Under stirring conditions: first add the fused magnesia particles into the mixer, then add a mixture that accounts for 55 to 57 wt % of the mixture, and stir for 10 to 15 minutes; then add the fused magnesia fine powder, Stir for 10 to 15 minutes, then add the rest of the mixture, and stir for 10...
Embodiment 2
[0061] A low-carbon magnesium-carbon refractory material added with magnesium silicon nitride powder and a preparation method thereof. The steps of the preparation method described in this embodiment are:
[0062] Step 1. Use 43-46wt% fused magnesia particles, 39-42wt% fused magnesia fine powder, 6.5-7.5wt% flake graphite, 5-5.5wt% phenolic resin and 3-4wt% Magnesium silicon nitride powder is used as raw material and ingredients.
[0063] Step 2. Add the magnesium silicon nitride powder into the phenolic resin in 3 to 5 times at 40 to 50° C. and under magnetic stirring conditions, and stir for 15 to 20 minutes each time to obtain a mixture, which is taken out for use.
[0064] Step 3. Under stirring conditions: first add the fused magnesia particles into the mixer, then add the mixture accounting for 57-59 wt% of the mixture, and stir for 10-15 min; then add the fused magnesia fine powder, Stir for 10 to 15 minutes, then add the rest of the mixture, and stir for 10 to 15 min...
Embodiment 3
[0069] A low-carbon magnesium-carbon refractory material added with magnesium silicon nitride powder and a preparation method thereof. The steps of the preparation method described in this embodiment are:
[0070] Step 1. Using 46-49wt% fused magnesia particles, 36-39wt% fused magnesia fine powder, 6-7wt% flake graphite, 4.5-5wt% phenolic resin and 4-5wt% nitriding Magnesium silicon powder is used as raw material and ingredients.
[0071] Step 2. Add the magnesium silicon nitride powder into the phenolic resin in 3 to 5 times at 40 to 50° C. and under magnetic stirring conditions, and stir for 15 to 20 minutes each time to obtain a mixture, which is taken out for use.
[0072] Step 3. Under stirring conditions: first add the fused magnesia particles into the mixer, then add a mixture that accounts for 59 to 61 wt % of the mixture, and stir for 10 to 15 minutes; then add the fused magnesia fine powder, Stir for 10 to 15 minutes, then add the rest of the mixture, and stir for ...
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