Banana peel yellow pigment and extraction method thereof
An extraction method, banana technology, applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve problems such as less research, and achieve the effect of reducing the degree of oxidation, high economic and social value, and reducing losses
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Embodiment 1
[0037] (1) Take 5 parts of fresh ripe bananas in parallel, remove the flesh and skin, wash the skin surface, scrape off the soft part of the inner layer of the skin, wash the jelly again, absorb the water, and chop it to a size of 0.3cm×0.3cm The fragments are ready for use, and the fragments are soaked in the color protection solution for 15 minutes. The color protection solution contains 0.05 (w / v)% sodium bisulfite, 0.1 (w / v)% vitamin C and 0.4 (w / v) % citric acid aqueous solution, pull out and pour water, place in the tetrapotassium pyrophosphate aqueous solution of 90 ℃, the concentration of tetrapotassium pyrophosphate aqueous solution is 0.4 (w / v)%, adjust pH value to be 2.5, 2.5, respectively with phosphate buffer. 6.5, 7, 8.5, 10, soak for 30 minutes, filter to get the filter residue for later use;
[0038] (2) Soak the filter residue in step (1) in ethanol and set the volume to 8 times the volume of the filter residue, ultrasonically extract in a constant temperature...
Embodiment 2
[0046](1) Take fresh ripe bananas, remove the flesh and skin, wash the skin surface, then scrape off the soft part of the inner layer of the skin, wash the jelly again, absorb the water, and chop it into 0.3cm×0.3cm pieces for later use. Submerge the fragments in the color protection solution for 15 minutes. The color protection solution is an aqueous solution containing 0.05% sodium bisulfite, 0.1% vitamin C and 0.4% citric acid. In the potassium aqueous solution, adjust the pH value to 6.5 with phosphate buffer solution, the concentration of the tetrapotassium pyrophosphate aqueous solution is 0.6%, soak for 40min, and filter to obtain the filter residue for later use;
[0047] (2) Soak the filter residue in step (1) in ethanol and set the volume to 8 times the volume of the filter residue, and take 7 parallel samples at 0°C, room temperature (25°C), 30°C, 40°C, 50°C , 80°C, 100°C constant temperature water bath conditions, ultrasonic extraction for 30min, the frequency is 3...
Embodiment 3
[0055] (1) Take fresh ripe bananas, remove the flesh and skin, wash the skin surface, then scrape off the soft part of the inner layer of the skin, wash the jelly again, absorb the water, and chop it into 0.3cm×0.3cm pieces for later use. Submerge the fragments in the color-protecting solution for 10 minutes. The color-protecting solution is an aqueous solution containing 0.05% sodium bisulfite, 0.1% vitamin C and 0.4% citric acid. In the potassium aqueous solution, adjust the pH value to 7 with phosphate buffer solution, the concentration of the tetrapotassium pyrophosphate aqueous solution is 0.7%, soak for 40min, and filter to obtain the filter residue for later use;
[0056] (2) Soak the filter residue in (1) in ethanol and set the volume to 10 times the volume of the filter residue, take 6 parallel sample solutions and extract 10, 20, 30, 40, 50 , 60min frequency is 50KHz, suction filtration, obtain extract, measure absorbance with UV-visible absorptiometry respectively a...
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