A kind of composite thermal fabric and preparation method thereof
A technology of fabrics and nanocomposite fibers, applied in textiles and papermaking, coating, electrospinning, etc., to achieve good application prospects, accelerate surface temperature, and effectively isolate toxic particles
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[0043] The present invention also provides a preparation method of the above-mentioned composite thermal fabric, the method comprising the following steps:
[0044] (1) Take graphene oxide and disperse it in deionized water; the graphene oxide is placed in deionized water, and ultrasonically dispersed for 40 to 50 minutes. The operating frequency during ultrasonic dispersion is 20 to 50kHZ, and the dispersion is completed to obtain graphene oxide dispersion liquid;
[0045] Preferably, the operating frequency during ultrasonic dispersion is 30-40kHZ.
[0046] (2) according to the required mass ratio, polyvinyl alcohol is dissolved in the graphene oxide dispersion of step (1) to swell, and the mass fraction of polyvinyl alcohol added is 5wt%~10wt% (and meets polyvinyl alcohol and The mass ratio of graphene oxide is 7:0.1~7:0.5.), swelling after adding for 45~55min;
[0047] Then heat at 90-100° C. for 3-5 hours, and cool to room temperature after heating to obtain a polyvinyl a...
Embodiment 1
[0061] A kind of nanocomposite fiber, described nanocomposite fiber is prepared from polyvinyl alcohol, polyethylene glycol and graphene oxide, wherein polyvinyl alcohol 6g, the mass ratio of described polyvinyl alcohol and polyethylene glycol is 2: 1. The mass ratio of polyvinyl alcohol to graphene oxide is 7:0.1, the total amount is 100g, and the balance is water. The electron microscope image of the obtained fiber is shown in figure 1 shown.
Embodiment 2
[0063] A kind of nanocomposite fiber, described nanocomposite fiber is prepared from polyvinyl alcohol, polyethylene glycol and graphene oxide, wherein polyvinyl alcohol 8g, the mass ratio of described polyvinyl alcohol and polyethylene glycol is 2.67: 1. The mass ratio of polyvinyl alcohol to graphene oxide is 7:0.1, the total amount is 100g, and the balance is water. The electron microscope image of the obtained fiber is shown in figure 2 shown.
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