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Low-expansion-coefficient insulating medium slurry and preparation method thereof

A low expansion coefficient, insulating medium technology, applied in the field of electronic materials, can solve the problems of rapid decline in glass comprehensive performance, difficulty in achieving low sintering temperature, and high processing temperature, and achieve excellent adhesion fastness and good acid and alkali corrosion resistance , the effect of low sintering temperature

Active Publication Date: 2019-12-10
航天科工(长沙)新材料研究院有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This technology improves upon existing methods such as solvent casting techniques and coating processes. These improvements include improved protection against environmental factors like acids (H2S) and bases due to their ability to resist erosion caused by these environments over longer periods of use without losing effectiveness. Additionally, this new method allows for precise control during manufacturing process while maintaining consistently strong bond between the material being applied onto the device's surfaces. Overall, it provides technical benefits with enhanced durability and reliance on electronic devices protected through various means including chemical vapor deposition (CVI).

Problems solved by technology

This patents discusses different methods used to prepare ceramic materials like AlN (aluminum oxynaphosphor). However, there may have issues related to these processes due to their lower thermal conductivity compared to traditional techniques involving firing at very high temperatures. Additionally, some manufacturing companies require specific conditions while producing certain types of material without sacrificially affecting them' quality. These technical challengings include ensuring proper matching between the refractory properties needed for optimal functioning of the final component made through the method described above, controlling the size of the starting components, maintaining consistency throughout the procedure, avoidance of defects caused by impurity particles, and achieving desired levels of mechanical stability over time.

Method used

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  • Low-expansion-coefficient insulating medium slurry and preparation method thereof
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  • Low-expansion-coefficient insulating medium slurry and preparation method thereof

Examples

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Embodiment 1

[0046] A low expansion coefficient insulating medium slurry and a preparation method thereof, the preparation steps are as follows:

[0047]a. Preparation of organic carrier: 1. by weight components, terpineol 60%, alcohol ester twelve 15%, butyl carbitol acetate 10%, butyl carbitol 7%, ethyl cellulose 8% Accurately weigh and put into a round bottom flask or dissolution kettle; ② Stir and dissolve at a constant temperature of 80-85°C for 3 hours to obtain a clear and transparent fluid;

[0048] b. Preparation of glass powder: ① mix silicon dioxide (SiO2) by weight component 2 )63%, alumina (Al 2 o 3 )18%, boron oxide (B 2 o 3 ) 9%, Calcium Oxide (CaO) 7%, Strontium Oxide (SrO) 1.5%, Zinc Oxide (ZnO) 1.5%, accurately weighed, and mixed evenly to form a mixed oxide; ②Put the mixed oxide into a platinum crucible , as for the high-temperature furnace, keep the temperature at 1650°C for 1 hour until the melting is uniform; ③ water quench the molten glass to obtain glass slag, ...

Embodiment 2

[0056] A low expansion coefficient insulating medium slurry and a preparation method thereof, the preparation steps are as follows:

[0057] a. Preparation of organic carrier: 1. by weight components, terpineol 55%, alcohol ester twelve 15%, butyl carbitol acetate 15%, butyl carbitol 7%, ethyl cellulose 8% Accurately weigh and put into a round bottom flask or dissolution kettle; ② Stir and dissolve at a constant temperature of 80-85°C for 3 hours to obtain a clear and transparent fluid;

[0058] b. Preparation of glass powder: ① mix silicon dioxide (SiO2) by weight component 2 )62%, alumina (Al 2 o 3 )17%, boron oxide (B 2 o 3 ) 10%, Calcium Oxide (CaO) 9%, Strontium Oxide (SrO) 0.5%, Zinc Oxide (ZnO) 1.5%, accurately weighed, and mixed evenly to form a mixed oxide; ②Put the mixed oxide into a platinum crucible , as for the high-temperature furnace, keep the temperature at 1650°C for 1 hour until the melting is uniform; ③quench the molten glass liquid with water to obtain...

Embodiment 3

[0065] A low expansion coefficient insulating medium slurry and a preparation method thereof, the preparation steps are as follows:

[0066] a. Preparation of organic carrier: 1. by weight components, terpineol 55%, alcohol ester twelve 15%, butyl carbitol acetate 16%, butyl carbitol 2%, ethyl cellulose 12% Accurately weigh and put into a round bottom flask or dissolution kettle; ② Stir and dissolve at a constant temperature of 80-85°C for 3 hours to obtain a clear and transparent fluid;

[0067] b. Preparation of glass powder: ① mix silicon dioxide (SiO2) by weight component 2 )74%, alumina (Al 2 o 3 )3%, boron oxide (B 2 o 3 ) 10%, calcium oxide (CaO) 9%, strontium oxide (SrO) 1%, flux 3%, accurately weighed, mixed evenly to form a mixed oxide; ② put the mixed oxide into a platinum crucible, and In the furnace, keep the temperature at 1650°C for 1 hour until the melting is uniform; ③quench the molten glass with water to obtain glass slag, and dry it; ④use the planetary ...

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Abstract

The invention provides low-expansion-coefficient insulating medium slurry. The low-expansion-coefficient insulating medium slurry is prepared from the following materials in percentage by weight: 8%-45% of an organic carrier, 55%-90% of glass powder, 0-5% of an auxiliary agent and 0-5% of a colorant; the organic carrier is prepared from the following materials in percentage by weight: 45%-60% of terpineol, 15%-25% of texanol, 5%-15% of butyl carbitol acetate,1%-10% of butyl carbitol and 4%-15% of ethyecellulose; and the glass powder is prepared from the following materials in percentage by weight: 50%-75% of silicon dioxide (SiO2), 10%-25% of aluminum oxide (Al2O3), 5%-15% of boron oxide (B2O3), 0-15% of calcium oxide (CaO), 0.1%-5% of strontium oxide (SrO), 0.1%-10% of zinc oxide (ZnO) and 0-5% of a fluxing agent. Glass glaze formed by the medium slurry has good acid and alkali corrosion resistance, good insulation, good water resistance and good gas resistance, a circuit on the surface of electronic ceramic can be effectively protected against corrosion damage, and short-circuiting or electric leakage of the circuit is prevented.

Description

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Claims

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Application Information

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Owner 航天科工(长沙)新材料研究院有限公司
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