Preparation method of hibiseu manihot perfume for tobaccos
A technology of tobacco spices and goldenflower sunflower, which is applied in the field of tobacco additives, can solve the problems of no goldenflower sunflower, etc., and achieve the effects of simple equipment, improved taste, and low production cost
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[0020] Example 1
[0021] Step Q1: Remove the surface impurities of fresh golden flower sunflower with intact skin and no insects, clean it with running water, and drain the body surface water.
[0022] Step Q2: Baking the cleaned sunflower at 60-70°C until its moisture content is 10-12%. After crushing through a 20-mesh sieve.
[0023] Step Q3: Put the dried golden sunflower powder into the barrel of the supercritical extraction kettle, set the temperature to 35°C, pressure to 15MPa, and carbon dioxide flow rate to 15L / h. At the same time, turn on the entrainer pump and inject 95% ethanol accurately and quantitatively. Entrainer, the mass ratio of dry sunflower powder to entrainer is 1:0.01, extraction is 2h, the fluid containing sunflower oil is collected from the outlet of the separation kettle, the extraction rate is 2.35%.
Example Embodiment
[0024] Example 2
[0025] Step Q1: Remove the surface impurities of fresh golden flower sunflower with intact skin and no insects, clean it with running water, and drain the surface water.
[0026] Step Q2: Spread the clean golden flower sunflower evenly on the tray, and leave it in a shaded and ventilated place for 20-28 hours. After the golden flower sunflower loses part of its moisture, move it to the sun for natural drying until it is dried. The moisture content of sunflower is 10-12%.
[0027] Of course, the speed of natural drying is related to the temperature, the intensity of the sun, the length of time, and the humidity of the air. The drying time needs to be adjusted according to the weather conditions of the time. Generally, it can be completed in 7-9 days. After crushing through a 20-mesh sieve.
[0028] Step Q3: Put the dried golden sunflower powder into the barrel of the supercritical extraction kettle, set the temperature to 40℃, pressure to 35MPa, and carbon dioxide f...
Example Embodiment
[0029] Example 3
[0030] Step Q1: Remove the surface impurities of fresh golden flower sunflower with intact skin and no insects, clean it with running water, and drain the body surface water.
[0031] Step Q2: Vacuum drying the clean golden flower sunflower, wherein the drying temperature is 60±2° C., the drying vacuum degree is -0.08±0.01 MPa, and the moisture content of the dried golden flower sunflower is 10-12%. After crushing through a 20-mesh sieve.
[0032] Step Q3: Put the dried golden sunflower powder into the cylinder of the supercritical extraction kettle, set the temperature to 50°C, pressure to 20MPa, and carbon dioxide flow rate to 8L / h. At the same time, turn on the entrainer pump and pour in 95% ethanol accurately and quantitatively. And propylene glycol mixture as entrainer, the mass ratio of dry sunflower powder to entrainer is 1:0.005, extraction is 4h, the fluid containing sunflower oil is collected from the outlet of the separation kettle, the extraction rate ...
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