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610results about How to "Low cost of preparation" patented technology

Preparation of microballoons based on microfluid

A microfluid-based microballoon preparation method adopts a microfluid channel system to lead a colloidal solution or a pre-polymer solution to form liquid drips in a mobile phase. The formation of the liquid drip-based template is used for bioanalysis and polymeric micro spheres of protein, gene and drug screening carrier. The preparation method includes the following steps: preparation of the microfluid channel: establishing a microfluid channel network by adopting the micro-machining technology or connecting a T-shaped channel with a pinhead, a polymer pipe and a tee joint (the channel is provided with two inlets, namely, a dispersed phase inlet and a continuous phase inlet and an outlet); preparation of the liquid drip template: encasing the two phase solutions of a dispersed phase solution and a continuous phase solution respectively into a pin case, connecting with the respective inlet, digital controlling an ejector jet pump to control the velocity of flow of the two phase solutions and acquiring even and stable liquid drip template from the outlet; preparation of the microballoon: drying and solidifying the liquid drip template and removing the impurities on the surface or inside to acquire a polymer microballoon according with the requirement of bioanalysis and protein, gene and drug screening carrier.
Owner:NANJING DONGJIAN BIOLOGICAL TECH

Single-crystal appearance layered nickel lithium manganate positive electrode material and preparation method thereof

The invention discloses a single-crystal appearance layered nickel lithium manganate positive electrode material and a preparation method thereof. The single-crystal appearance layered nickel lithiummanganate positive electrode material is prepared by the following preparation method with the steps of (1) performing preparation to obtain nickel manganese precursors by using nickel salts and manganese salts by a wet chemical method, wherein the mol ratio of the Ni to Mn is 1:1; (2) performing pre-sintering on the nickel manganese precursors to obtain the nickel manganese oxide precursors; (3)mixing the nickel manganese oxide precursors with Li source and M source additives; then, performing calcination to obtain the single-crystal appearance layered nickel lithium manganate positive electrode material. The advantage that the single crystal particle has the theory density is sufficiently achieved, so that the compaction density of an electrode plate made of positive electrode materialscan be improved, so that the volume energy density of a lithium ion battery is improved. The defects inside the single crystal particles can be greatly reduced; the structure stability of the positive electrode material in the charging and discharging process can be effectively improved, so that the service life of the lithium ion battery is prolonged.
Owner:GUANGDONG BRUNP RECYCLING TECH +1

Hydro-fining catalyst roasted at low temperature and preparation method thereof

The invention discloses a hydro-fining catalyst roasted at a low temperature and a preparation method thereof. The preparation method comprises the following steps of: taking aluminum hydroxide dry glue or modified aluminum hydroxide dry glue as a raw material to prepare a catalyst carrier, then impregnating metal active components in VIB and VIII groups and preparing the hydro-fining catalyst through drying and roasting. The content of an alumina carrier is 60-90 weight percent, the content of metallic oxide in the VIB group is 5-35 weight percent, and the content of metallic oxide in the VIII group is 1-10 weight percent. An activity phase of the catalyst has proper stacking layer number and film crystal length, the interaction between the carrier and metal is reduced, the better dispersion state of the active components can be kept, and the HDS (Hydro-desulfurization) ability of sulfide difficult to remove in an oil product is improved. The hydro-fining catalyst is particularly suitable for the hydro-desulfurization of naphtha, the hydro-fining of inferior diesel oil and the hydro-treatment of FCC (Fluid Catalytic Cracking) raw materials or hydro-cracking raw materials and other distillate oil.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Preparation method for biomass medicinal charcoal

The invention discloses a preparation method for biomass medicinal charcoal, which belongs to the technical field of processing and preparation of activated charcoal, and aims to reduce ash content in activated charcoal and to improve adsorption performance of the activated charcoal. The method comprises the following steps: crushing biomass and screening the biomass with a 20 to 200 mesh sieve; carrying out pickling and alkali washing on the biomass after screening and removal of impurities; drying the biomass; sending the raw material of the treated biomass to an activation furnace, heating the raw material to a temperature of 300 to 600 DEG C under the protection of nitrogen and carrying out carbonization for 30 to 240 minutes; allowing carbon dioxide to enter into the activation furnace at a temperature of 800 to 1000 DEG C, carrying out carbonization for 30 to 360 minutes, with gas flow being 10 to 300 L/h, and after carbonization, cooling the biomass to room temperature so as to obtain the biomass medicinal charcoal. Ash content, decolouring capacity and adsorption quantity of the prepared biomass medicinal charcoal are all superior to those of wooden activated charcoal; the biomass medicinal charcoal has the advantages of a simple operation process, low cost, suitability for large scale production and strong market competitiveness.
Owner:QINGDAO UNIV OF SCI & TECH

Preparation method of manganese molybdate microcrystal

The invention which belongs to the inorganic non-metallic material preparation field especially relates to a preparation method of a manganese molybdate (W-MnMnO4) microcrystal. The method comprises the following steps: mixing a soluble manganese salt and sodium molybdate which are treated as raw materials according to a certain molar ratio, carrying out stirring reacting for 5-30min at 20-50DEG C, and carrying out a hydrothermal reaction for 6-48h at 160-230DEG C; and naturally cooling to room temperature after finishing the hydrothermal reaction, filtering, washing, and drying to obtain the manganese molybdate microcrystal. The soluble divalent manganese salt of the invention is a mixture of above one or above two of manganese chloride, manganese nitrate and manganese acetate. The preparation method has the advantages of simple and easily implemented process, high purity, low impurity content, good dispersibility, and low cost; and the diameter and the length of the obtained product are 10-50mum and 100-300mum respectively. The manganese molybdate microcrystal prepared in the invention can be widely applied to the electronic and electrical field, the mechanical field, the chemical engineering field, the building field and the like, and is an excellent predecessor for preparing other manganese salt functional materials.
Owner:BOHAI UNIV

Random copolymer containing biphenyl structural polyether sulfone and polyether ketone sulfone and preparation method thereof

The invention relates to a random copolymer containing biphenyl structural polyether sulfone and polyether ketone sulfone and a preparation method thereof, and belongs to the field of high molecular materials. The preparation method comprises the following steps: using 4,4'-dichlorodiphenyl sulfone, 4,4'-dihydroxy biphenyl and 4,4'-dihydroxy diphenyl ketone as raw materials, anhydrous potassium carbonate as salt forming agent, N-methyl ketopyrrolidine or cyclobutyl sulfone as solvent, and methylbenzene or dimethyl benzene as water carrier; adding the raw materials, the salt forming agent, the solvent and the water carrier into a container provided with a mechanical stirrer and a thermometer, under the protection of nitrogen, heating the mixture to reflow with water, vaporizing redundant water carrier, and reacting the mixture for 4 hours at a temperature of between 160 and 240 DEG C to obtain a coarse product; and boiling the coarse product with ethanol or acetone, filtering the mixture, boiling the filtrate with distilled water, filtering the mixture, and drying the sediment to obtain a refined polymer product. The polymer has good compatibility for polyaryletherketone and polyarylethersulfone; and the preparation method is simple and convenient and has low cost.
Owner:JILIN UNIV

Preparation method of vinyl sulfate

The invention relates to a preparation method of vinyl sulfate. The preparation method comprises the following steps: adding ethylene glycol into a reaction kettle A filled with a halohydrocarbon solvent, uniformly stirring, dropwise adding thionyl chloride to carry out a substitution reaction, removing hydrogen chloride by reduced-pressure distillation, then, washing a reaction solution to be neutral by using a saturated sodium bicarbonate solution, standing still, and skimming to obtain a glycol sulfite halohydrocarbon solution; adding the glycol sulfite halohydrocarbon solution into a reaction kettle B, adding monopotassium phosphate or sodium tungstate as a catalyst, regulating the pH by using a sodium bicarbonate aqueous solution, and adding a sodium hypochlorite aqueous solution to carry out an oxidation reaction; at the end of the reaction, skimming to obtain a vinyl sulfate halogenated alkane solution, carrying out concentration, then, adding n-hexane to carry out recrystallization, and carrying out filtration to obtain high-purity vinyl sulfate. By using the preparation method, raw materials are available, the price of the catalyst is low, the product is easy to purify, and the obtained product is low in acidity, low in water content, high in purity and suitable for large-scale production.
Owner:ZHUHAI SMOOTHWAY ELECTRONICS MATERIALS

Preparation method of standard spectrum sample

Belonging to the field of metallurgical sample detection, the invention relates to a preparation method of a standard spectrum sample. The method includes the processes of: component selection, preparation of a standard sample through a continuous casting middle ladle top pouring method, stability investigation and conclusion. The method is characterized in that the process of preparing the standard sample by the continuous casting middle ladle top pouring method comprises the steps of: model baking, sample model establishment, sample model pouring by the top pouring method, demolding, segmentation and surface treatment, physical property detection, surface treatment, chemical component uniformity test, and fixed value analysis. The standard sample prepared in the invention not only satisfies the standard sample requirements in terms of physical property, texture, component range and uniformity, but also has reduced preparation cost and increased sampling number. At least 200 pieces can be prepared every time, thus being over 20 times as many as a model casting sampling number. And the preparation number can satisfy the current production requirements. Thus, the standard sample preparation method of the invention boasts very high practical value.
Owner:SHANXI TAIGANG STAINLESS STEEL CO LTD

Tissue engineering double-layered tubular support and preparation method thereof

The invention relates to a tissue engineering double-layered tubular support and a preparation method thereof. The support is composed of two polymer layers with different pore structures, the inner layer is a compact nanofiber structure, and the outer layer is of a porous nanofiber structure. The preparation method comprises the following steps of: dissolving a polymer material in a solvent, pouring in a mould, performing phase separation overnight, demoulding to obtain a polymer gel, performing solvent replacement, and freeze drying to obtain a nanofiber tubular support with a compact structure; sleeving the nanofiber tubular support on a mould stem to obtain a casting mould; and dissolving a polymer material in a solvent, casing the polymer solution in the casing mould by combing an electroporation technology, performing phase separation overnight, demoulding, performing solvent replacement, removing the solvent and/or porogen, and freeze drying to obtain the tissue engineering double-layered tubular support. The preparation method disclosed by the invention is simple in operation, free of complicated equipment, suitable for large-scale production and low in preparation cost; the whole mechanical property of the support is improved by introducing other polymers in the phase separation system.
Owner:DONGHUA UNIV

Marine organism fermentation fertilizer and preparation method thereof

The invention discloses a marine organism fermentation fertilizer and a preparation method thereof. The marine organism fermentation fertilizer comprises the following components in parts by weight: 10-15 parts of a humic acid, 30-50 parts of shell powder, 20-40 parts of slit powder in a culture pond, 3-10 parts of a polypeptide amino acid, 12-14 parts of decaying manure, 5-10 parts of tea seed cakes subjected to tea saponin removing and degreasing, 0.5-1.5 parts of silicate bacteria, and 3-5 parts of strong brine. The marine organism fermentation fertilizer and the preparation method have the advantages that raw materials are wide in source, the preparation cost is low, and secondary pollution is avoided during the production process; the bioactivity is higher, the nutrient is more complete, and besides medium trace elements such as calcium, magnesium, zinc and silicon, the marine organism fermentation fertilizer is rich in natural organic nutrients such as nitrogen, phosphorus, potassium and the amino acid and the humic acid, is wide in use range, can be used as an acid soil conditioner, can also be used as a calcicolous and magniferous crop supplement trace element, and can be further used as a water quality improver and a fertilizer agent.
Owner:THE FIRST INST OF OCEANOGRAPHY SOA

Method for preparing lithium silicate serving as high-temperature CO2 absorbing material

The invention discloses a method for preparing lithium silicate material absorbing high-temperature CO2 by taking artificial zeolite as raw material, and provides a process for preparing lithium silicate material serving as high-temperature CO2 absorbent by use of artificial zeolite. Lithium silicate precursors are prepared from LiNO3 and artificial zeolite in different proportions by ion exchange and sol-gel methods, and the lithium silicate material is synthesized by roasting the lithium silicate precursors at a temperature between 600 and 900 DEG C for 2 to 8 hours. The lithium silicate material prepared absorbs CO2 in a thermogravimetric analyzer at a temperature between 400 and 700 DEG C in CO2 and N2 atmosphere in different proportions. Aiming at the problem of a great amount of high-temperature CO2 emitted from power plants and flue gas, the method recycles carbon resources and reduces CO2 emission. The method synthesizes the lithium silicate material by taking cheap artificial zeolite and LiNO3 as raw material and adopting the ion exchange and sol-gel methods. Compared with the prior art, the method has the advantages of cheap and readily available artificial zeolite used as the raw material, reduction in preparation cost of the lithium silicate material and easiness of realizing industrial production.
Owner:KUNMING UNIV OF SCI & TECH

Method of repairing agricultural soil by calcium peroxide-charcoal

The invention discloses a method of repairing agricultural soil by calcium peroxide-charcoal. The method of repairing the agricultural soil by the calcium peroxide-charcoal is characterized in that acharcoal raw material is washed to remove materials adhering on the surface and then dried naturally, and then broken; the broken charcoal is put in a pyrolyzing furnace for sealing and pyrolyzation;the charcoal after pyrolyzation is wrapped and formed by plastic mesh fabrics with pore diameters, and an active filler of charcoal is made and placed in the soil to be repaired; the calcium peroxideis dissolved in water, the pH value of the calcium peroxide is adjusted, leachate of the calcium peroxide is prepared to spray the soil to be repaired regularly, and the purpose of removing heavy metals and organic pollutants in the soil is finally achieved by combined treatment of the charcoal and the calcium peroxide. The method of repairing the agricultural soil by the calcium peroxide-charcoalis low in cost, the raw materials are easy to obtain, action time is long, the applicable pH range is wide, the heavy metals and the organic pollutants in the soil can be repaired, the soil fertilitycan be improved, and the method of repairing agricultural soil by calcium peroxide-charcoal is suitable for remediation of contaminated agricultural soil.
Owner:DONGHUA UNIV
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