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results about "Diphenyl ketone" patented technology
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Dibenzyl ketone, or 1,3-diphenylacetone, is an organic compound composed of two benzyl groups attached to a central carbonyl group.
A method for preparing a phenylalkylamine compound
Active
CN117304051B
reduce usage
avoid expensive
Ptru catalyst
Organic synthesis
The application provides a preparation method of a
benzaldehyde
aniline
compound and relates to the technical field of
organic synthesis
. The preparation method provided by the application comprises the following steps: in a
solvent
, with an alkali as a
promoter
, under an
atmosphere
with an
oxygen
concentration of 20v100%, the temperature of a
reaction system
is controlled to be 50-70 DEG C, a
diphenyl ketone
compound I is reacted with an
aniline
compound II to generate a
benzaldehyde
aniline
compound III, and the
reaction product
is subjected to
column chromatography
separation to obtain a pure
benzaldehyde
aniline compound III. The method has the beneficial effects that the reaction is simple, green and environment-friendly, the use of an expensive
transition metal
catalyst is avoided, the reaction condition is mild and controllable, and an environment-friendly byproduct is generated.
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Owner:
NANCHANG UNIV
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