Ceramic matrix composite thermo-mechanical damage characterization method based on micro-porosity increment
A composite material and microporous technology, which is applied in the field of damage tolerance evaluation and design of ceramic matrix composite materials, can solve the problems of inaccurately characterizing the thermomechanical damage of CMCs, and achieve the effect of accurate evolution behavior
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Embodiment 1
[0068] S11: Heat the muffle furnace to 1100°C, then quickly place the CMCs specimen in the furnace and keep it warm for 10-20 minutes. In this embodiment of the present invention, 10 minutes is taken as an example to make the temperature of the specimen uniform and fully establish thermal balance with the furnace;
[0069] Then quickly take the test piece out of the furnace, put it in a constant temperature water bath of distilled water at 25°C, and keep stirring the distilled water to avoid the accumulation of the vapor layer, so that the test piece can fully exchange heat with the distilled water;
[0070] Cool the test pieces in a water bath to room temperature, take them out and dry them in the air, and number each test piece;
[0071] The open porosity and pore size distribution of each specimen before and after cyclic thermal shock were determined by mercury intrusion porosimetry using a mercury porosimeter, and the presence of CMCs in the specimen was observed by X-ray ...
Embodiment 2
[0073] S11: Heat the muffle furnace to 800°C, then quickly place the CMCs specimen in the furnace and keep it warm for 10-20 minutes. In this embodiment of the present invention, 20 minutes is taken as an example to make the temperature of the specimen uniform and fully establish thermal balance with the furnace;
[0074] Then quickly take the test piece out of the furnace, put it in a constant temperature water bath of distilled water at 25°C, and keep stirring the distilled water to avoid the accumulation of the vapor layer, so that the test piece can fully exchange heat with the distilled water;
[0075] Cool the test pieces in a water bath to room temperature, take them out and dry them in the air, and number each test piece;
[0076] The open porosity and pore size distribution of each specimen before and after cyclic thermal shock were determined by mercury intrusion porosimetry using a mercury porosimeter, and the presence of CMCs in the specimen was observed by X-ray c...
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Abstract
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