Method for producing silicon single crystal
A manufacturing method and technology of single crystal silicon, applied in the direction of single crystal growth, single crystal growth, chemical instruments and methods, etc., can solve problems such as easy occurrence of dislocations
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[0065] [1] When red phosphorus is used as a dopant
[0066] The resistivity was controlled by adding a red phosphorus dopant according to the position of the straight body length of the silicon single crystal 10 , and pulling of the silicon single crystal 10 doped with red phosphorus was performed simultaneously.
[0067] The diameter of the straight body of the single crystal silicon 10 is set to be 301 mm or more and 330 mm or less. In the embodiment, a crucible 3 with an inner diameter of 22 inches (558.8 mm) is used (the inner diameter of the crucible 3 / the straight body diameter of the single crystal silicon = 1.86). In the example, a crucible 3 with an inner diameter of 32 inches (812.8 mm) was used (the inner diameter of the crucible 3 / the diameter of the straight body of the single crystal silicon = 2.70).
[0068] In the example, the rotation speed of the crucible 3 was set to 16 rpm when the shoulder portion of the silicon single crystal 10 started to form, and was c...
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