Antioxidant moistening lipstick containing lycium pigment and sea buckthorn oil and preparation method of lipstick
A technology of wolfberry pigment and sea buckthorn oil is applied in the directions of medical preparations containing active ingredients, cosmetic preparations, preparations for skin care, etc. Thick and sticky feeling and other problems, to achieve excellent moisturizing protection effect, good moisturizing antioxidant effect, and comprehensive effect
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Embodiment 1
[0054] Preparation of red wolfberry pigment:
[0055] (1-1) Put 10g of shredded Lycium barbarum in the mortar;
[0056] (1-2) Add 15mL of petroleum ether-ethanol mixture to the shredded wolfberry, grind it into a paste, let it stand for several minutes, transfer the extract to a separating funnel, and repeat three times; the petroleum ether-ethanol Petroleum ether and ethanol in the mixed solution are mixed with a volume ratio of 3:2, and both petroleum ether and ethanol are analytically pure;
[0057] (1-3) Add 10ml of saturated NaCl solution to the extract, discard the water layer, and wash the organic layer twice with 10mL of distilled water; transfer the washed organic layer to a dry Erlenmeyer flask, add anhydrous sodium sulfate to dry half Hour;
[0058] (1-4) filter the dried organic layer into a round bottom flask, distill, and concentrate to 1 mL;
[0059] (1-5) Chromatography: ① Construction of the chromatographic column: Weigh 30g of neutral alumina and slowly add ...
Embodiment 2
[0063] Preparation of black wolfberry pigment:
[0064] (2-1) Weigh the black wolfberry and grind it in an agate mortar, and the ground black wolfberry powder is passed through a 60-mesh sieve;
[0065] (2-2) Add petroleum ether to the sieved black wolfberry as a degreasing solvent, perform ultrasonic degreasing for 30 minutes at a solid-liquid ratio of 1:20 (g / mL), repeat twice, and dry to remove petroleum ether;
[0066] (2-3) Accurately weigh 50 g of degreased black wolfberry dry powder, add ethanol with a concentration of 60% according to a solid-liquid ratio of 1:15 (g / mL), in a water bath at 50° C., ultrasonicate for 25 minutes, and repeat the operation three times;
[0067] (2-4) The black wolfberry treated with 60% ethanol sonication was concentrated to 1-2 mL by rotary steaming.
Embodiment 3
[0069] Preparation of sea buckthorn oil:
[0070] (3-1) cleaning the seabuckthorn fruit to remove impurities;
[0071] (3-2) Dry the washed sea buckthorn fruit at 65°C for 8 hours, take it out and cool it;
[0072] (3-3) The cooled seabuckthorn fruit is pulverized and passed through a 60-mesh sieve to obtain the seabuckthorn fruit dry powder;
[0073] (3-4) Take 10.00 g of seabuckthorn fruit dry powder and place it in a Soxhlet extractor, and add petroleum ether according to a solid-liquid ratio of 1:8 (g / mL);
[0074] (3-5) Extract with water for 3 hours in an 80°C water bath to obtain an extract;
[0075] (3-6) suction-filtering the extracted seabuckthorn fruit powder, and merging the extract;
[0076] (3-7) Distilling the combined extract under reduced pressure;
[0077] (3-8) The distillate is centrifuged at 9350r / min to obtain seabuckthorn oil.
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