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Detection pretreatment method and detection method of water-based adhesive for cigarettes

A water-based glue for cigarettes, a technology to be detected, applied in measuring devices, instruments, scientific instruments, etc., can solve problems such as emulsification and inaccurate detection results of plasticizers, and achieve guaranteed accuracy, strong anti-pollution, and instrument sensitivity. high effect

Active Publication Date: 2020-06-19
CHINA TOBACCO HENAN IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, surfactants have both hydrophobic and hydrophilic groups. When testing water-based rubber for tobacco with high surfactant content, the existing pre-testing methods will emulsify during the extraction process, resulting in abnormal test results. The detection result of the plasticizer in the tobacco water-based adhesive is inaccurate

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  • Detection pretreatment method and detection method of water-based adhesive for cigarettes

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Embodiment Construction

[0047] Various exemplary embodiments of the present invention will now be described in detail. It should be noted that unless specifically stated otherwise, the relative arrangement of components and steps, numerical expressions and numerical values ​​set forth in these embodiments do not limit the scope of the present invention.

[0048] The following description of at least one exemplary embodiment is actually only illustrative, and in no way serves as any limitation to the present invention and its application or use.

[0049] The technologies, methods, and equipment known to those of ordinary skill in the relevant fields may not be discussed in detail, but where appropriate, the technologies, methods, and equipment should be regarded as part of the specification.

[0050] In all examples shown and discussed herein, any specific value should be interpreted as merely exemplary, rather than as a limitation. Therefore, other examples of the exemplary embodiment may have different va...

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Abstract

The invention discloses a detection pretreatment method and detection method of a water-based adhesive for cigarettes , the method comprises the following steps: mixing cigarette water-based adhesive,an extractant and a dispersant, and carrying out vortex oscillation for a period of time to obtain an extract liquid; adding inorganic salt into the extracting solution, oscillating for a period of time, centrifuging and taking supernatant; and filtering the supernatant to obtain a to-be-detected solution. Inorganic salt is added in the liquid-liquid extraction process, and the emulsification phenomenon caused by a surfactant is destroyed by utilizing the hydrophilicity and dissociation effect of inorganic salt ions, so that a dispersing agent and an extracting agent are well layered, and theaccuracy of a detection result is guaranteed.

Description

Technical field [0001] The present invention relates to the field of cigarette water-based glue detection, and more specifically, to a pretreatment method and detection method for cigarette water-based glue detection. Background technique [0002] Cigarette water-based glue is an indispensable material for cigarette production. The pre-treatment method for the detection of water-based gum for cigarettes is as follows: Weigh a sample of water-based gum in a triangular flask, add dispersant water and extractant, shake and extract for 30 minutes, pipette an appropriate amount of extract into a centrifuge tube, and centrifuge and take the supernatant. GC / MS analysis. [0003] In the production process of tobacco water-based glue, an appropriate amount of surfactant is usually added to meet the needs of the sizing process. Surfactants have both hydrophobic and hydrophilic groups. When testing cigarette water-based gums with a high content of surfactants, the existing pre-testing metho...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02G01N30/06G01N30/72
CPCG01N30/02G01N30/06G01N30/7206G01N2030/045G01N2030/062
Inventor 王鹏飞潘立宁孙学辉孙志涛段鹍席高磊赵声辰聂聪李明哲杨松王宏伟
Owner CHINA TOBACCO HENAN IND