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Preparation method of high-hardness and high-transparency polyimide coated ultrathin glass

A polyimide, ultra-thin glass technology, applied in the field of display screen, can solve the problem of unable to meet the needs of mobile phone folding screen or curling screen, and achieve the effect of high flexibility, high transparency, and convenient process operation

Pending Publication Date: 2020-06-23
JIANGHAN UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0013] The invention provides a method for preparing ultra-thin polyimide-coated glass with high hardness and high transparency. The technical problem of curly screen requirements has realized the technical effect of convenient process operation and simple process, and the produced transparent polyimide glass composite film meets the bending and folding requirements of flexible screens

Method used

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  • Preparation method of high-hardness and high-transparency polyimide coated ultrathin glass
  • Preparation method of high-hardness and high-transparency polyimide coated ultrathin glass
  • Preparation method of high-hardness and high-transparency polyimide coated ultrathin glass

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preparation example Construction

[0049] See attached figure 1 with 2 A method for preparing high-hardness and high-transparency polyimide-coated ultra-thin glass provided by the present invention comprises the following steps:

[0050] S1: Preparation of thin glass by overflow down-draw method;

[0051] S2: Thin glass is heated and stretched in the first, second and third stages by multiple high-temperature tension rollers;

[0052] S3: cooling the thin glass through several tension rollers to obtain glass film;

[0053] S4: coating the slurry of transparent polyimide on the glass film;

[0054] S5: After the glass film is dried, a finished product of a transparent polyimide glass composite film is formed.

[0055] Further, step S1 is specifically:

[0056]Using the overflow down-draw method, the raw materials are mixed according to the set ratio, and melted to make molten glass; the molten glass flows into the overflow tank through the platinum channel after being stirred and clarified; when the molten ...

Embodiment 1

[0068] S1: The raw materials are mixed according to the set ratio by the overflow pull-down method, and melted to make molten glass; the molten glass flows into the overflow tank through the platinum channel after being stirred and clarified; after the molten glass overflows, it flows from both sides of the overflow tank The overflow flows down evenly along the conical part of the overflow tank, merges together at the lower part of the conical shape, and pulls down to form a large piece of glass, which forms a thin glass during the continuous stretching process; the thickness of the thin glass is 220um.

[0069] S2: The thin glass passes through the first high-temperature tension roller for secondary heating, and the temperature is controlled at 110°C above the glass transition temperature; the second high-temperature tension roller is used to stretch and thin the thin glass, reducing the thickness of the thin glass to 42um. The thin glass passes through the third high-temperat...

Embodiment 2

[0075] S1: The raw materials are mixed according to the set ratio by the overflow pull-down method, and melted to make molten glass; the molten glass flows into the overflow tank through the platinum channel after being stirred and clarified; after the molten glass overflows, it flows from both sides of the overflow tank The overflow flows down evenly along the conical part of the overflow tank, merges together at the lower part of the conical shape, and pulls down to form a large piece of glass, which forms a thin glass during the continuous stretching process; the thickness of the thin glass is 240um.

[0076] S2: The thin glass passes through the first high-temperature tension roller for secondary heating, and the temperature is controlled at 130°C above the glass transition temperature; the second high-temperature tension roller is used to stretch and thin the thin glass, reducing the thickness of the thin glass to 44um. The thin glass passes through the third high-temperat...

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Abstract

The invention relates to a preparation method of high-hardness and high-transparency polyimide film-coated ultrathin glass. The preparation method comprises the following steps: preparing thin glass by adopting an overflow down-drawing method; heating, stretching and thinning the thin glass in a first stage, a second stage and a third stage through a plurality of high-temperature tension rollers;cooling the thin glass through a plurality of tension rollers to obtain a glass film; coating the transparent polyimide slurry on the glass film; and drying the glass film to form a finished product of the transparent polyimide glass composite film. The preparation method is convenient in technological operation and simple in process, and the produced transparent polyimide glass composite film meets the bending and folding requirements of a flexible screen.

Description

technical field [0001] The invention relates to the technical field of display screens, in particular to a method for preparing high-hardness and high-transparency polyimide-coated ultra-thin glass. Background technique [0002] With the rapid development of flexible displays, the application scenarios of flexible displays are becoming more and more clear. Portable large-screen mobile phones may be the biggest demand spot in the market: the cover and substrate of folding mobile phones must be flexible and can be bent, rolled and folded arbitrarily. Its service life is required to be folded more than 200,000 times, that is, within 5 years, it can be folded 100 times a day, and there is no obvious crease when it is folded and unfolded. The specific requirements are: [0003] (1) Good flexibility and ductility, the flexibility of the cover plate and substrate can be expressed by bending radius and folding radius. The bending radius of flexible glass is 1-5mm, and the folding ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B17/06C03C17/32
CPCC03B17/064C03B17/068C03C17/32C03C2217/78C03C2218/32
Inventor 尤庆亮刘继延刘志宏
Owner JIANGHAN UNIVERSITY