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501 results about "Glass composites" patented technology

Large-size metallic glass composite material with tensile ductility and preparation method thereof

InactiveCN102181809ARealize one-step moldingUniform Work Hardening AbilityGlass compositesWork hardening
The invention discloses a large-size metallic glass composite material with tensile ductility and a preparation method thereof. A composition expression of the metallic glass composite material is ZraTibMcCudNieBef (atom percent), wherein M is one of Nb, V or Hf, a is not less than 10 and not more than 70, b is not less than 10 and not more than 70, c is not less than 4 and not more than 20, d isnot less than 2 and not more than 20, e is not less than 0 and not more than 15, f is not less than 5 and not more than 22.5, and a+b+c+d+e+f is equal to 100. The preparation method is called after semi-solid progressive solidification method, which comprises the following steps of: smelting master alloy ingots and casting into master alloy profiles; putting the master alloy profiles into a crucible and heating until the profiles are completely melted, and performing the overheating processing to dissolve impurity phases; reducing the temperature to a solid-liquid two-phase region; performingsemi-solid processing, and controlling the shape and the size of a precipitated solid solution phase; and then performing the semi-solid progressive solidification to form the large-size metallic glass composite material with tensile ductility. By adopting the method, the homogeneous and defect-free large-size (30 mm) metallic glass composite material is prepared, and the composite material has remarkable work hardening capacity and excellent tensile strength and ductility.
Owner:NANJING UNIV OF SCI & TECH

Gelatine/biological activity glass composite sponge dressing and preparation thereof

The present invention relates to a gelatin / biological activity glass compounded sponge dressing and a preparation method thereof, belonging to the biomaterial field. The dressing is characterized in that a solution of a content of between 1 and 30 percent is prepared with gelatin as the raw material; the biological activity glass powder with a weight percentage of between 2 and 20 percent, prepared by the fusion method or the sol-gel method, is put into the solution; and then a mixed solution is obtained by magnetic stirring. The mixed solution is poured into a mould, the liquid layer is up to between 1 and 8 mm, the mixed solution is kept stand for 0.5 to 3 h, and then the prefreezing temperature is controlled between 20 DEG C below zero and 80 DEG C below zero; the lyophilization is controlled to be carried out at a temperature of 40 DEG C below zero and a pressure of between 5 and 10 KPa. The section of the present invention is of a double layer composite structure with a thickness of between 0.5 and 5 mm, wherein, the upper layer is a loose porous layer, and the lower layer is a dense powder layer, the thickness of the powder layer being up to between 0.1 and 2.0 mm. The double layer sponge dressing is flexible, which can be used as a parenchyma wound restoring material. Particularly, the double sponge dressing is suitable for any one of parenchyma ulcers of cervix erosions, oral ulcers, bedsores, sinuses, fat liquescency wounds, venereal disease ulcers, hemorrhoids, diabetes ulcers, etc. and the long-term erosions thereof.
Owner:上海硅健生物材料有限公司

Lithium disilicate glass-ceramics composite material using ZrO2 as reinforcing phase and method for making same

InactiveCN101139170AGuaranteed densificationGood mechanical propertiesGlass particleMechanical property
The present invention relates to a lithium disilicate glass-ceramic composite material with ZrO2 as the reinforcing phase and thepreparation method, which solve the problems that the production cycle is long, the cost is high, the products can be easily formed and the mechanical properties of the lithium disilicate glass-ceramic is lower. The present invention is composed of the lithium disilicate base glass and zirconia powders. The preparation method goes in that the ball milling is carried out according to the components of the original glass; the desiccated raw materials are placed in a corundum crucible so as to be melted under high temperature; the glass solution is poured into the distilled water to go into water quenching so as to be changed into 1 to 2mm glass particles; the ball milling is applied to the glass particles after going into the water quenching so as to obtain the glass powders; the lithium disilicate glass powder is taken to be mixed with the zirconia powders and the ball milling is applied to the lithium disilicate glass powder and the zirconia powders with the alcohol as the medium; the vacuum heating-press sintering is implemented and then the lithium disilicate glass-ceramic composite material with ZrO2 as the reinforcing phase is prepared. The present invention is uneasily deformed, has short production cycle and low cost and has excellent bending strength and fracture toughness indexes.
Owner:HARBIN INST OF TECH

Porous ceramic-microcrystalline glass composite insulation decorative plate and preparation method thereof

The invention discloses a porous ceramic-microcrystalline glass composite insulation decorative plate and a preparation method thereof. The porous ceramic comprises ceramic tile raw material, additive, pore forming agent and foaming agent, and the microcrystalline glass comprises SiO2, CaO, ZnO, Al2O3, Na2O, K2O, etc. The preparation method comprises the following steps: firstly uniformly mixing ceramic tile raw material, additive, pore forming agent and foaming agent, and conducting ball milling to obtain an ultrafine powder slurry; then granulating, drying, and conducting compression molding; drying the green ware body and then sintering in a roller kiln or a shuttle kiln; then, melting quartz sand, limestone, soda ash and other minerals or chemical raw materials to obtain a glass melt, carrying out water quenching on the glass melt to obtain glass particles; screening the dried glass particles and then classifying, paving on the surface of a porous ceramic plate, then pushing into a crystallization kiln to sinter, crystallize, anneal and cool the glass particles to form a microcrystalline glass layer; in the process, simultaneously compounding the microcrystalline glass with the porous ceramic plate to form the porous ceramic-microcrystalline glass composite insulation decorative plate.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Conductive paste for solar cell and preparation method thereof

The invention provides a conductive paste and a preparation method thereof. The conductive paste comprises aluminum powder, an inorganic binding agent, an organic carrier and metal-glass composite powder, wherein the metal-glass composite powder is of nano-particles and a core-shell structure, glass is used as a core material, and metal is used as a shell material. The conductive paste disclosed by the invention is good in storage stability and less prone to sedimentation and agglomeration, and the conductive paste is less prone to leakage from a screen during screen printing; after sintering, an aluminum film is smooth in surface and grey white, and has no aluminum vesicles or aluminum beads; and furthermore, the part in contact and superimposition with a back silver electrode, of the aluminum film is wiped by a non-dust cloth, and wiping traces and powder dropping can be avoided. The series resistance of the produced solar cell is reduced obviously, a filling factor is increased obviously, and the average photoelectric conversion efficiency of a monocrystalline silicon cell piece can be above 18.20%. Simultaneously, the conductive paste disclosed by the invention is good in construction performance, a film layer formed after sintering is compact, the sintering thickness is uniform, the bending of a silicon chip is small, the sheet resistance is small and the open circuit voltage (Voc) of the formed cell is high.
Owner:BYD CO LTD

Low-temperature co-fired microwave dielectric ceramic material and preparation method thereof

A low-temperature, high stability co-fired microwave dielectric composite of ceramic and glass, including 85-99 wt % microwave dielectric ceramic of formula [1-y-z[(1−x)Mg2SiO4−xCa2SiO4]−yCaTiO3−zCaZrO3, wherein 0.2≦x≦0.7,0.05≦y≦0.3 and 0.02≦z≦0.15], and 1 to 15 wt % with Li2O—BaO—SrO—CaO—B2O3—SiO2 glass respectively made at a low sintering temperature of ceramic for co-firing with Ag or Cu electrode, employing eutectic phase of ceramic oxides to reduce its melting temperature, a low melting-point glass material with high chemical stability as a sintering aid added to oxides and raw material powders of Li2O, BaO, SrO, CaO, B2O3 and SiO2, obtained by combining and melting the ingredients in the temperature range between 1000 to 1300° C., quenching and crashing, and then adding it to the main ceramic oxides to form the final composition. This ceramic/glass composite material may be co-fired with an Ag and Cu electrode at 900° C.-970° C. for 0.5-4 hours in a protective atmosphere. After sintering, this dielectric material possesses efficacious microwave dielectric properties, dielectric constant between middle-K to low-K at 815, high quality factors, low dielectric loss, low temperature-capacitance coefficient and superior chemical stability suitable for manufacture of multilayer ceramic devices.
Owner:WALSIN TECHNOLOGY CORPORATION
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