Long laminate, method for producing same, and printed wiring board
A manufacturing method and a laminated body technology, which are applied in the manufacture of printed circuit precursors, printed circuits, printed circuits, etc., can solve the problems of low dimensional stability of fluororesin films, and achieve thin film and signal transmission, dimensional stability and Excellent folding resistance
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[0302] Hereinafter, the present invention will be described in detail through examples, but the present invention is not limited thereto.
[0303] Examples 1-15, 19, and 20 are examples, and examples 16-18 are comparative examples.
[0304] (The ratio of each unit in the fluoropolymer)
[0305] The ratio of the NAH unit in the fluoropolymer is determined by the following infrared absorption spectrum analysis. The ratio of units other than NAH units was determined by melt NMR analysis and fluorine content analysis.
[0306] (Infrared absorption spectroscopic analysis)
[0307] The fluoropolymer was press-molded to obtain a film with a thickness of 200 μm. The film was analyzed by infrared spectroscopy to obtain an infrared absorption spectrum. In the infrared absorption spectrum, the absorption peak of the NAH unit in the fluoropolymer appears at 1778cm -1 . To measure the absorbance of the absorption peak, use the molar absorptivity of NAH 20810mol -1 ·L·cm -1 The rati...
manufacture example 1
[0362] The methyl ethyl ketone of the nonionic surfactant of the resin powder P-1 of 120g, 12g (Nios Co., Ltd. manufacture, Ftergent710FL), the methyl ethyl ketone of 234g is dropped in the horizontal ball mill, with the zirconium bead of diameter 15mm the resin powder P-1 was dispersed to obtain a liquid composition. Use a die coater to coat the liquid composition on the surface of the long strip of copper foil-1 in a roll-to-roll manner, dry it at 100°C for 15 minutes under a nitrogen atmosphere, and then dry it at 350°C under a nitrogen atmosphere. After firing for 5 minutes, annealing was performed to obtain a long copper foil-1 with a fluororesin layer. The results are shown in Table 2.
manufacture example 2
[0364] A long copper foil-2 with a fluororesin layer was obtained in the same manner as in Production Example 1 except that the thickness of the fluororesin layer was changed. The results are shown in Table 2.
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