Unlock instant, AI-driven research and patent intelligence for your innovation.

Production method of disperse dye blue B56#

A production method and technology for dispersing blue, applied in anthracene dyes, organic dyes, chemical instruments and methods, etc., can solve the problems of raw material waste, environmental pollution, waste of raw materials, etc., and achieve the effect of reducing the discharge of three wastes

Active Publication Date: 2020-09-22
YANGZHOU RIXING BIO TECH
View PDF7 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This new method uses special chemicals called benfblue bile acids that break down certain compounds found naturally or artificialally into smaller molecules like pigments. These small particles are then separated from other substances during processing steps such as drying processes. By doing this, they become useful products made up mostly of these tiny parts without being thrown away after use.

Problems solved by technology

This patented technical problem addressed in this patents relates to producing high purity dyestuffs with minimal harmful chemical substances during manufacturing processes such as one described earlier. Existing methods involve sending excessive amounts of material away from the main facility or burning them off at an expensive cost. Additionally, some techniques have been developed but are still being researched due to their negative impact on human health caused by these solvents.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Production method of disperse dye blue B56#
  • Production method of disperse dye blue B56#

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of production method of dye disperse blue B56#, by utilizing sodium sulfite to treat 1-aminoanthraquinone DMF residue to purify and produce mixed nitrate, then the mixed nitrate is sequentially passed through mononitration, mononitration refining, condensation, dinitration, hydrolysis, reduction and In the process of bromination transformation, the product disperse blue B56# is finally obtained; the mother liquor recovered by hydrolysis is reprocessed to recover the by-product 2,4-dinitrophenol.

[0022] The reprocessing of the recovered mother liquor by hydrolysis specifically includes the following steps:

[0023] (1) adding the mother liquor recovered by hydrolysis into the refining kettle, slowly adding mass fraction of 98% sulfuric acid at room temperature to adjust the solution to a pH value of 5, the amount of sulfuric acid is 45% of the quality of the mother liquor recovered by hydrolysis; then adjust the reaction temperature to 65°C, The reaction time is...

Embodiment 2

[0029] A kind of production method of dye disperse blue B56#, by utilizing sodium sulfite to treat 1-aminoanthraquinone DMF residue to purify and produce mixed nitrate, then the mixed nitrate is sequentially passed through mononitration, mononitration refining, condensation, dinitration, hydrolysis, reduction and In the process of bromination transformation, the product disperse blue B56# is finally obtained; the mother liquor recovered by hydrolysis is reprocessed to recover the by-product 2,4-dinitrophenol.

[0030] The reprocessing of the recovered mother liquor by hydrolysis specifically includes the following steps:

[0031] (1) adding the reclaimed mother liquor by hydrolysis to the refining kettle, slowly adding mass fraction of 90% sulfuric acid at room temperature to adjust the solution to a pH value of 7, the amount of sulfuric acid is 50% of the quality of the reclaimed mother liquor by hydrolysis; then adjust the reaction temperature to 60°C, The reaction time is 0...

Embodiment 3

[0035] A kind of production method of dye disperse blue B56#, by utilizing sodium sulfite to treat 1-aminoanthraquinone DMF residue to purify and produce mixed nitrate, then the mixed nitrate is sequentially passed through mononitration, mononitration refining, condensation, dinitration, hydrolysis, reduction and In the process of bromination transformation, the product disperse blue B56# is finally obtained; the mother liquor recovered by hydrolysis is reprocessed to recover the by-product 2,4-dinitrophenol.

[0036] The reprocessing of the recovered mother liquor by hydrolysis specifically includes the following steps:

[0037] (1) adding the mother liquor recovered by hydrolysis to the refining kettle, slowly adding mass fraction of 95% sulfuric acid at room temperature to adjust the solution to a pH value of 5, the amount of sulfuric acid is 45% of the quality of the mother liquor recovered by hydrolysis; then adjust the reaction temperature to 70°C, The reaction time is 1...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a production method of disperse dye blue B56#, and belongs to the technical field of chemical dye. The method comprises the following steps: treating 1-aminoanthraquinone DMF residues with sodium sulfite to purify and produce mixed nitrate, and sequentially carrying out primary nitrification, primary nitrification refining, condensation, secondary nitrification, hydrolysis,reduction and bromination transformation on the mixed nitrate to finally obtain the product disperse blue B56#; and retreating the hydrolysis recovery mother liquor to recover a byproduct that is 2,4-dinitrophenol. According to the invention, 2,4-dinitrophenol sodium salt is produced in a filter cake hydrolysis process of product disperse blue B56#l; the 2,4-dinitrophenol sodium salt is dissolvedin the hydrolysis recovery mother liquor in order to effectively utilize effective components in the hydrolysis recovery mother liquor and reduce the emission of three wastes, the byproduct 2,4-dinitrophenol is produced through acidification and filtration, and the byproduct detection meets the standard, so that the byproduct can be used as an enterprise raw material for producing coating intermediates.

Description

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Owner YANGZHOU RIXING BIO TECH
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More