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2371 results about "Sulphate sodium" patented technology

Anti-bacterial hand-washing solution and preparation method thereof

The invention specifically relates to an anti-bacterial hand-washing solution and a preparation method thereof, belonging to the field of washing agents. The anti-bacterial hand-washing solution is mainly composed of fatty alcohol polyoxyethylene ether sodium sulfate, cocoamidopropyl betaine, alkyl glucoside, polyquaternary ammonium salt, fatty glyceride, humectant, mixed plant extract, tetrasodium ethylenediamine tetraacetate, sodium chloride, citric acid, jojoba oil, 1,2-pentanediol and essence. The preparation method comprises the following steps: dissolving fatty alcohol polyoxyethylene ether sodium sulfate, cocoamidopropyl betaine and fatty glyceride with water with a total amount of 70 to 80%; uniformly mixing jojoba oil, polyquaternary ammonium salt, humectant and alkyl glucoside; and mixing two mixed solutions obtained in the previous two steps, adding the rest components and carrying out uniform mixing under stirring. The anti-bacterial hand-washing solution provided by the invention has skin-care, skin-moistening, antibacterial, bacteriostatic, anti-allergy, soothing, anti-inflammatory and hand-microcirculation-improving effects and is a multifunctional hand-washing solution with strong sterilization and detergency capabilities and substantial skin-care and skin-moistening effects.
Owner:WALCH GUANGZHOU COMMODITY

Method for preparing asymmetric nanofiltration membrane by blending polyether sulfone and sulfonated polysulfone high polymers

The invention discloses a method for preparing an asymmetric nanofiltration membrane by blending polyether sulfone and sulfonated polysulfone high polymers. A blending nanofiltration membrane with an asymmetric structure is prepared in one step by the nanofiltration membrane through a phase transformation method. The method comprises the following steps of: preparing casting membrane liquid, namely mixing the polyether sulfone, the sulfonated polysulfone high polymers, an additive and a solvent to prepare the casting membrane liquid; and forming a membrane by the phase transformation method, wherein the membrane comprises a flat membrane and a hollow fibrous membrane. The interception rate of the nanofiltration membrane to 0.5 to 1.5 g/L sodium chloride and 0.5 to 1.5 g/L sodium sulfate under the operating pressure of between 0.1 and 0.8 MPa is between 20 and 95 percent, the interception rate of the nanofiltration membrane to polyethylene glycol with the relative molecular mass of between 600 and 2,000 is between 40 and 99.9 percent, and the pure water flux of the membrane is between 10 and 250 L/(m2hbar). The asymmetric nanofiltration membrane of the invention has the advantages of high strength and toughness, high compactness resistance, chlorine resistance and high-temperature resistance, and can be applied to aspects of water treatment, wastewater treatment, material separation and the like.
Owner:天津森诺过滤技术有限公司

Method for preparing modified polyamine porous starch

The invention relates to a method for preparing modified polyamine porous starch obtained through the following steps: preparing starch as the raw material and compound enzymes into porous starch; cross-linking the porous starch; modifying the porous starch through etherification; and grafting different polyamine molecules. The modified polyamine porous starch is capable of absorbing AG25 and AR18 in wastewater by the hollow structure and grafted functional groups thereof, particularly, the removal rate of both AG25 and AR18 in the wastewater is higher than 98% according to the tests; the modified polyamine porous starch can be taken out and dipped in a sodium sulfate solution with the molar concentration thereof being 0.05mol/L to 1mol/L for desorption when the absorption effect is reduced, particularly, the desorption rate of AG25 and AR18 is higher than 90%; and the absorption effect of the modified polyamine porous starch is not reduced after being subjected to desorption and analysis for multiple times. Compared with the common porous starch, the product of the invention increases the absorption capacity by more than two times and ensures the high selectivity. Therefore, the method of the invention is of significant economic and social benefits and is applicable to the absorption treatment of heavy-metal ions and wastewater containing various dyes in the industries, such as printing and dyeing, textile and cosmetics.
Owner:TONGJI UNIV +1

Method for catalyzing dynamic kinetic resolution of arylamine via racemization catalyst

The invention discloses a method for catalyzing dynamic kinetic resolution of arylamine via a racemization catalyst, comprising the following steps of: 1) adding p-chlorophenol, n-pentanoic acid, dicyclohexylcarbodiimide and 4-dimethylamino-pyridine, and carrying out mixing, filtration, drying, concentration and column chromatography to obtain a pentanoic acid p-chlorophenyl ester acyl donor; 2) carrying out coprecipitation on magnesium chloride solution and aluminum chloride solution and carrying out water-heat treatment to obtain chloridion intercalated hydrotalcite, adding the chloridion intercalated hydrotalcite in lauryl sodium sulfate aqueous solution, and carrying out backflow, cooling, centrifugation, water washing, acetone washing and drying to obtain a carrier; 3) adding palladium salt and the carrier, and carrying out heating, ascorbic acid addition, centrifugation, water washing, acetone washing and freeze-drying to obtain the racemization catalyst; and 4) adding arylamine, the acyl donor, lipase and the racemization catalyst in toluene and placing in a stainless steel reactor to add hydrogen so as to obtain amide. The method provided by the invention is used for catalyzing the dynamic kinetic resolution of arylamine, has rapid reaction rate, low temperature, high conversion rate and high product optical purity, and has great application value.
Owner:ZHEJIANG UNIV

Preparation method for 4-methyl-5-ethyoxyl-oxazole

The invention relates to a preparation method for 4-methyl-5-ethyoxyl-oxazole. The preparation method for the 4-methyl-5-ethyoxyl-oxazole comprises the following steps of: performing cyclization reaction on N-ethoxyl oxalyl alanine ethyl ester under the action of phosphorus oxychloride/triethylamine/dimethylformamide used as a cyclization dehydrating agent at the temperature of between 40 and 60 DEG C for 0.5 to 1 hour; heating to 75 to 100 DEG C and reacting for 5 to 10 hours; hydrolyzing the reaction materials and separating out a water layer; adding an aqueous solution of sodium hydroxide into an organic layer to hydrolyze, adjusting the pH value to be 12 to 14, distilling to obtain ethanol and adjusting the pH value to be 2.0 to 3.0 by adding sulfuric acid; heating to 65 DEG C to perform decarboxylation; adjusting the pH value to 8.0 to 10.0 by using alkali; after chloroform extraction, drying the organic layer by using anhydrous sodium sulfate; and distilling the chloroform under normal pressure to obtain the target product 4-methyl-5-ethyoxyl-oxazole. The process is easy to operate and by the preparation method, industrialized production is easy to realize; the reaction condition is mild, side reaction is few, reaction yield is high and the product content is high; and toxic methylbenzene is not used, so physical health of staff and environmental protection are facilitated.
Owner:HUBEI HUISHENG PHARMA
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