The invention relates to the related technical field of electrochemical electrodes, and discloses a preparation process and a use method of an electrochemical
composite electrode, and the preparation process comprises the following steps: S1, weighing a certain amount of materials according to a
mass ratio of a piezoelectric material to PVDF (or P (VDF-TrFE)) of 1: 20-4: 1, dissolving and dispersing in N, N-
dimethylformamide, N, N-
dimethylformamide, N, N-
dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, the preparation method comprises the following steps: adding PVDF (or P (VDF-TrFE)) into a mixture of one or more polar
organic liquids such as N, N-
dimethylacetamide,
dimethyl sulfoxide and the like, stirring or ultrasonically dispersing uniformly to prepare a PVDF (or P (VDF-TrFE)) solution with the
mass percent of 5-20%; the
composite electrode provided by the invention is low in production cost, simple in preparation method and easy to amplify to realize industrial production, the electro-catalytic performance of the
composite electrode in circulating
water treatment is remarkably improved through an optimized heat treatment process, and the
electrode shows higher electrochemical efficiency in treatment of industrial
wastewater containing high-concentration organic pollutants and has good application prospects. And the service life is prolonged to 6000 hours, and is prolonged by 20% compared with the service life of a traditional
electrode.