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Ejector for interfacial polymerization reaction

An interfacial polymerization and ejector technology, applied in chemical instruments and methods, filtration loops, feeding devices, etc., can solve the problem of affecting the formation of diaphragms, the inability of fresh solution to be replenished quickly, and the inability of low-concentration solutions and other derivatives to quickly carry To ensure uniformity and improve efficiency

Active Publication Date: 2020-10-02
SHANDONG JOZZON MEMBRANE TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a jet device for interfacial polymerization reaction, aiming to solve the problem that the existing film-making equipment cannot quickly take the reacted low-concentration solution and other derivatives away from the reaction area, and the fresh solution cannot be quickly supplied to the reaction area , thus affecting the problem of diaphragm forming

Method used

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  • Ejector for interfacial polymerization reaction
  • Ejector for interfacial polymerization reaction
  • Ejector for interfacial polymerization reaction

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] refer to Figure 1-3 As shown, an ejector for interfacial polymerization reaction includes a solution tank 1, a partition 2, a circulation device 3 and a guide roller 4, and the partition 2 is fixedly installed in the solution tank 1 and divides the solution tank 1 into an upper tank 101 1, the upper and lower parts of the lower groove 102, the partition plate 2 is provided with a number of wing-like structures 201 connecting the upper groove 101 and the lower groove 102, and the front end of the partition plate 2 is provided with an opening 202 connecting the upper groove 101 and the lower groove 102; The rollers 4 are installed in a linear array on the top of the upper tank 101 of the solution tank 1, a passage for the membrane 7 to pass is formed between the guide roller 4 and the separator 2, the bottom of the lower tank 102 of the solution tank 1 is provided with a circulation inlet 103, and the upper part is provided with a Circulation outlet 104;

[0023] The wi...

Embodiment 2

[0029] As a preferred embodiment of the present invention, this embodiment adds a flanging mechanism on the basis of the first embodiment.

[0030] refer to figure 2 and Figure 4 As shown, in order to make the diaphragm 7 only have one side contacting the solution to participate in the interface reaction, a kind of jet device for the interface polymerization reaction includes the flange plate 5, the flange plate 5 is two inclined plates, and the flange plate 5 is fixedly installed on On the inner wall of the upper groove 101 below the joint of the guide roller 4 rotating shaft and the upper groove 101, and the flanging plate 5 is located above the dividing plate 2;

[0031] Under the common clamping and limiting of the guide roller 4 and the inclined flange plate 5, the diaphragm 7 forms a groove-like structure, so that only one side of the diaphragm 7 participates in the interface reaction to form a high polymer layer. After the reaction, the solution and flocculation The...

Embodiment 3

[0033] As a preferred embodiment of the present invention, this embodiment adds a circulating liquid outlet pipe 6 on the basis of the second embodiment.

[0034] refer to figure 1 and Figure 5 As shown, in order to increase the flow rate of the solution, a jet device for interfacial polymerization, the circulation outlet 104 in the lower tank 102 of the solution tank 1 is connected with a circulation outlet pipe 6 full of hole-shaped nozzles 601, and the circulation outlet Tube 6 is a T-shaped tube.

[0035] In order to intensify the flow velocity of the solution in the lower tank 102, the solution that the circulation pump 302 is allowed to beat enters the lower tank 102 of the solution tank 1 through the circulation outlet pipe 6 that is full of hole-shaped nozzles 601, thus increasing the flow velocity of the solution and making the upper The discharge speed of the reacted solution and flocculent impurities in the tank 101 is accelerated, and new solution is quickly rep...

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Abstract

The invention discloses an ejector for interfacial polymerization reaction, and relates to the technical field of interfacial polymerization layer preparation equipment. The ejector comprises a solution tank, a partition plate, a circulating device and guide rollers, the partition plate is fixedly installed in the solution tank and divides the solution tank into an upper tank and a lower tank, thepartition plate is provided with a plurality of wing-shaped structures communicating with the upper tank and the lower tank, and the front end of the partition plate is provided with an opening communicating with the upper tank and the lower tank; the guide rollers are mounted at the top of the upper tank of the solution tank in a linear array, a circulating inlet is formed in the bottom of the lower tank of the solution tank, and a circulating outlet is formed in the side part of the lower tank of the solution tank; the circulating device comprises a circulating pipeline and a circulating pump, one end of the circulating pipeline communicates with the circulating inlet, and the other end communicates with the circulating outlet; and the circulating pump is connected to the circulating pipeline in series, and a filter is arranged on the circulating pipeline. The solution participating in the reaction and flocculent impurities generated by the reaction can be rapidly discharged, and anew solution can be rapidly and uniformly supplemented, so that the efficiency of the interfacial polymerization reaction is remarkably improved.

Description

technical field [0001] The invention relates to the technical field of interface polymerization equipment, in particular to a fluidizer for interface polymerization. Background technique [0002] Regarding the application of interfacial polymerization technology to prepare reverse osmosis membranes, the conventional preparation equipment is to set up two dipping tanks, which hold the oil phase solution and the water phase solution respectively. a polymer. Part of the polymer is attached to the surface of the basement membrane to form a desalination layer, and the other part is suspended in the solution in the form of flocculent impurities. [0003] How to quickly let the reacted solution and the flocculent impurities produced by the reaction leave the basement membrane, and quickly and evenly replenish the unreacted solution to the basement membrane surface has been a problem that has been explored in the industry. The current common practice in the industry is to circulat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J4/00B01D67/00B01D61/02B01D69/12B01D36/00
CPCB01D36/00B01D61/025B01D69/125B01J4/002
Inventor 张辉王肃星魏忠武李振宁
Owner SHANDONG JOZZON MEMBRANE TECH