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Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles and preparation method and quality control method thereof

A kind of granule and diamond technology, which is applied in the field of Zhuang medicine gold mother granule and its preparation, can solve the problems such as the report of the preparation method and quality control method of Zhuang medicine gold mother granule that have not been found yet

Pending Publication Date: 2020-10-30
GUANGXI UNIV OF CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] So far, no report has been found on the Zhuang medicine gold mother granule and its preparation method and quality control method

Method used

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  • Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles and preparation method and quality control method thereof
  • Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles and preparation method and quality control method thereof
  • Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles and preparation method and quality control method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0058] The preparation of embodiment 1 Zhuang medicine gold master granule

[0059] As shown in Table 1, get 9 medicinal materials and put them into a multifunctional extraction pot, heat and reflux with 60% ethanol to extract twice, each time for 45 minutes, add 60% ethanol for the first time according to the ratio of material to liquid=1:10, the second time Next, add 60% ethanol according to the ratio of solid to liquid = 1:8. Combine the extracts, filter, recover the ethanol from the filtrate until it has no alcohol smell, concentrate the filtrate to a concentrated solution with a relative density of 1.08 (60°C), weigh and record the concentrated solution, extract an appropriate amount of concentrated solution to measure the solid content, according to the formula " Total solid content = solid content rate × total weight of the concentrated solution" to calculate the total solid content in the concentrated solution, add auxiliary materials to the concentrated solution accor...

Embodiment 2

[0060] Example 2 Pharmacodynamics Study of Zhuang Medicine Jinmu Granules on SPID Rats

[0061] 1. Materials

[0062] 1.1 Experimental animals

[0063] Ninety SPF-grade female SD rats, weighing (200±20) g, were purchased from Hunan Slake Jingda Experimental Animal Co., Ltd., and were bred in the animal room of Guangxi University of Traditional Chinese Medicine. Certificate number: SCXK Xiang (2019-0002), room temperature 20-25°C, humidity 40%-70%, adaptive feeding for 7 days before the experiment, mice free access to food and water.

[0064] 1.2 Drugs and reagents

[0065] Zhuang medicine Jinmu granules were prepared according to the method in Example 1, batch number: G20190601; Huahong granules were purchased from Huahong Pharmaceutical Co., Ltd., batch number: 20180403; compound dexamethasone acetate tablets were purchased from Nanguo Pharmaceutical Co., Ltd., batch number: 171202; Bacterial solution: The mixed bacterial suspension provided by the Department of Microbiolo...

Embodiment 3

[0101] Example 3 Qualitative Identification of Main Components in Zhuang Medicine Golden Mother Granules

[0102] 1. Experimental materials

[0103] 1.1 Experimental Instruments

[0104] KQ3200B ultrasonic cleaner, Kunshan Ultrasonic Instrument Co., Ltd.; HWS-26 electric heating constant temperature water bath, Shanghai Qixin Scientific Instrument Co., Ltd.; JM-A5002 electronic balance, Zhuji Chaoze Weighing Equipment Co., Ltd.; DGG-9426A Electric constant temperature blast drying oven, Shanghai Qixin Scientific Instrument Co., Ltd.; SQP electronic balance, Sartorius Scientific Instrument (Beijing) Co., Ltd.; ZF-20C dark box ultraviolet analyzer, Shanghai Baoshan Gucun Electro-optical Instrument Factory; 98 -1-B electronic thermostat heating mantle, Tianjin Tester Instrument Co., Ltd.; TLC silica gel G plate, Qingdao Ocean Chemical Co., Ltd.; TLC silica gel G plate, Qingdao Jiyida Silicone Reagent Co., Ltd. ; P-1 TLC expansion cylinder, Shanghai Xinyi Instrument Factory Co.,...

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Abstract

The invention relates to the field of medicine preparation, in particular to Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles and a preparation method and a quality control method thereof. The Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles are prepared from the following raw materials in parts by weight: 545-565 parts of Smilax scobinicaulis, 545-565parts of Polygonum sinense L., 545-565 parts of rhizoma smilacis glabrae, 545-565 parts of whitebackleaf mallotus root, 434-454 parts of sargentgloryvine stem, 360-380 parts of giant knotweed rhizome, 323-343 parts of lightyellow sophora root, 323-343 parts of amur corktree bark and 323-343 parts of japanese violet herb or root. The Zhuang medicine Smilax scobinicaulis and Polygonum sinense L. particles can effectively inhibit the increase of the number of white blood cells and the number of neutrophils in SPID rats and improve the conditions of uterus adhesion, epithelial cell proliferationin pathological sections and the like of the SPID rats, and has no influence on immune organs.

Description

technical field [0001] The invention relates to the field of medicine preparation, in particular to gold mother granules of Zhuang medicine, a preparation method and a quality control method thereof. Background technique [0002] The prescription of Zhuang medicine Jinmu granules is optimized on the basis of the prescription of the patented Zhuang medicine Fuyajing granules. Mainly composed of Gaeuginhgangh (strong medicine name) King Kong thorn (Chinese medicine name), Gaeumei (strong medicine name) Huotanmu (Chinese medicine name), Gaebengzlaz (strong medicine name) Daxueteng (Chinese medicine name), Godienggangh (strong medicine name) Polygonum cuspidatum ( Chinese medicine name), Gaeulanghauh (Chinese medicine name), Smilax tuckahoe (Chinese medicine name), Godungzhau (Chinese medicine name) Baibeiyegen (Chinese medicine name) and other Zhuang medicine materials. It has the functions of clearing away heat and poison, dehumidifying and stopping leucorrhea, and can be use...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/896A61K36/90A61K9/16A61K47/36A61P15/00A61P29/00G01N30/90G01N30/02
CPCA61K9/1652A61K36/185A61K36/47A61K36/489A61K36/704A61K36/756A61K36/86A61K36/896A61K36/90A61P15/00A61P29/00G01N30/02G01N30/90A61K2300/00
Inventor 王志萍冯桥王孝勋陈俊黎芳谢谭芳李晓霞蒋雅娴苏佳昇
Owner GUANGXI UNIV OF CHINESE MEDICINE
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