A kind of cosmetic plastic injection material and its injection method
A technology of water for injection and L-polylactic acid, applied in the field of biomedical engineering, can solve the problems of waste of manpower and material resources, short residence time, multiple injections, etc., and achieve the effect of saving materials and costs, strong hydrophilicity, and avoiding injections
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Embodiment 1
[0037] A modified L-lactic acid plastic material, characterized in that: The modified L-lactic acid plastic material is first obtained by the copolymerization reaction of poly 2-hydroxysuccinic acid and L-polylactic acid, and then modified Mix L-lactic acid with sodium hyaluronate and mannitol to get it.
[0038] The preparation steps of modified L-polylactic acid are specifically:
[0039] a, the synthesis of poly 2-hydroxysuccinic acid:
[0040] a 1 , under nitrogen protection atmosphere, at first in reactor, add the 2-hydroxysuccinic acid of 40 weight parts, and add the diisopropyl titanate of chelation type two (acetylacetonate group) as catalyst, catalyst bis(acetylacetonate) Base) diisopropyl titanate consumption is 0.1% of the moles of 2-hydroxysuccinic acid;
[0041] a 2 , Then the temperature in the reactor is raised to 110°C, and the esterification and polycondensation reaction is carried out at a stirring speed of 80r / min under normal pressure, and the reaction ...
Embodiment 2
[0058] A modified L-lactic acid plastic material, characterized in that: The modified L-lactic acid plastic material is first obtained by the copolymerization reaction of poly 2-hydroxysuccinic acid and L-polylactic acid, and then modified Mix L-lactic acid with sodium hyaluronate and mannitol to get it.
[0059] The preparation steps of modified L-polylactic acid are specifically:
[0060] a, the synthesis of poly 2-hydroxysuccinic acid:
[0061] a 1 , under the nitrogen protection atmosphere, at first in the reactor, add the 2-hydroxysuccinic acid of 45 weight parts, and add the diisopropyl titanate of chelation type two (acetylacetonate group) titanate as catalyst, catalyst bis(acetylacetonate) Base) diisopropyl titanate consumption is 0.12% of the moles of 2-hydroxysuccinic acid;
[0062] a 2 , Then the temperature in the reactor was raised to 118°C, and the esterification and polycondensation reaction was carried out at a stirring speed of 100r / min under normal pressu...
Embodiment 3
[0079] A modified L-lactic acid plastic material, characterized in that it is composed of a modified L-lactic acid plastic material. The modified L-lactic acid is mixed with the modified L-lactic acid, sodium hyaluronate and mannitol.
[0080] The preparation steps of modified L-polylactic acid are specifically:
[0081]a, the synthesis of poly 2-hydroxysuccinic acid:
[0082] a 1 , under nitrogen protection atmosphere, at first in reactor, add the 2-hydroxysuccinic acid of 50 weight parts, and add the diisopropyl titanate of chelation type two (acetylacetonate group) as catalyst, catalyst bis(acetylacetonate) Base) diisopropyl titanate consumption is 0.15% of the moles of 2-hydroxysuccinic acid;
[0083] a 2 , Then, the temperature in the reactor was raised to 125°C, and the esterification and polycondensation reaction was carried out at a stirring speed of 120r / min under normal pressure, and the reaction time was 5h;
[0084] a 3 , when the temperature at the top of th...
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