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329results about How to "Uniform cells" patented technology

Water-based ultra-thin fire-retardant coating for steel structures and preparation method of fire-retardant coating

The invention discloses a water-based ultra-thin fire-retardant coating for steel structures. The fire-retardant coating comprises components as follows: a binder emulsion, an intumescent flame retardant system, filler, deionized water and additives, wherein the additives comprise a dispersing agent, an antifoaming agent, a mold inhibitor, an anti-flash-rust agent, a coalescing agent, a leveling agent and a thickener; the intumescent flame retardant system comprises a dehydration catalyst, a carbonizing agent and a foaming agent. The invention further designs a preparation method of the water-based ultra-thin fire-retardant coating for the steel structures. The components are mixed sequentially to be prepared into the water-based ultra-thin fire-retardant coating for the steel structures in a vertical sand mill and a dispersing tank. The prepared coating is large in adhesive force, high in hardness, good in fireproof property, good in anti-scratch performance and excellent in weather resistance and water resistance, the surface layer of the coating is fine and smooth, the decoration performance is improved significantly, and the preparation method is low in energy consumption and has the advantages that the harm to human bodies and the pollution to the environment during preparation are small and the like.
Owner:JIANGSU MARINE VICTORY COATING

Expandable polypropylene beading, preparation method thereof, and its foaming beading and foaming molding products

The invention provides an expandable polypropylene bead and a preparation method of the expandable polypropylene beads, and also provides foaming beads and foaming molding products of the expandable polypropylene beads, which relates to the resin expandable beads technical field. Random copolymerized polypropylene is used as basic resin, so that melting intensity can reach to an ideal range when in foaming with high melting intensity polypropylene and low density polyethylene resin being added. Expandable beads are prepared in a closed reactor without external pressure with pentane being used as foaming agent. The expandable beads contain 1 to 15 parts by weight of the high melting intensity polypropylene, 1 to 10 parts by weight of the low density polyethylene, 1.0 to 3.8 parts by weight of the foaming agent and 0.1 to 10 parts by weight of nucleating agent on the basis of 100 parts by weight of the random copolymerized polypropylene. The expandable polypropylene beads are easy to foam, whose foaming rate can reach to 16 times with uniform cells and whose foam volume weight is about 0.05 to 0.12g/cm3. The invention adopts a low-pressure method to produce the polypropylene foaming products in different shapes according to the requirement with low equipment requirement and low cost.
Owner:CHINA PETROLEUM & CHEM CORP +1

Thermoplastic polyurethane elastomer foam bead and preparation method thereof

The invention discloses a thermoplastic polyurethane elastomer foam bead and a preparation method thereof. The method comprises the following steps: firstly, adding thermoplastic polyurethane particles and water to a reaction kettle according to the mass ratio of 1 to (0.8-4); adding liquid carbon dioxide to the reaction kettle, and controlling the intensity of pressure and the temperature in the reaction kettle, so that the carbon dioxide in the reaction kettle is in a super-critical state; raising the temperature inside the reaction kettle to 90-140 DEG C; carrying out heat preservation; putting the materials in the kettle into a pressure tank, maintaining pressure, and cooling to below 70 DEG C; foaming the thermoplastic polyurethane elastomer particles once, and controlling the volume ratio of the reaction pressure to the pressure tank to be 1 to (15-30); putting the disposable foam particles into a storage tank, and carrying out secondary normal pressure foaming to obtain thermoplastic polyurethane elastomer foam beads; and removing the surface moisture of the foam beads, and curing the foam beads at normal pressure and normal temperature for over 48 hours, so as to obtain the product. The product disclosed by the invention has the characteristics of even and compact cells, small size, high percentage of closed area, high molding product strength, good rebound resilience and the like.
Owner:新辉新材料(常州)有限公司

Polyvinyl alcohol-polyurethane elastic buffing wheel and preparation method thereof

The invention discloses a polyvinyl alcohol-polyurethane elastic buffing wheel and a preparation method of the polyvinyl alcohol-polyurethane elastic buffing wheel. The preparation method comprises the steps that firstly, polyvinyl alcohol is mixed with distilled water, and the mixture is dissolved for 20-30 minutes under the condition of 50-95 DEG C water bath and at the rotation speed of 400-600r/min to obtain a polyvinyl alcohol aqueous solution; then, the polyvinyl alcohol aqueous solution is heated up to 30-100 DEG C, grinding materials are firstly added into the polyvinyl alcohol aqueous solution, after the mixture of the grinding materials and the polyvinyl alcohol aqueous solution is stirred and mixed evenly at the rotation speed of 400-600r/min, polyurethane pre-polymers, catalysts and air hole generating agents are added, and all the components are stirred and mixed evenly at the rotation speed of 400-600r/min and react for 5-10min; solidification is conducted for 2-4h under the condition of 30-100 DEG C, and then the buffing wheel which is good in elasticity, good in water resistance, good in heat-dissipating performance and high in mechanical strength is obtained. The elastic buffing wheel is even in foam hole, good in abrasion resistance and grinding force, not prone to deforming or curling in humid environment and applicable to long-time grinding work.
Owner:SOUTH CHINA UNIV OF TECH

Method for preparing microcrystalline foam glass by using high titanium blast furnace slag and waste glass powder

The invention discloses a method for preparing microcrystalline foam glass by using high titanium blast furnace slag and waste glass powder. The method comprises the following steps: grinding the high titanium blast furnace slag and waste glass powder, uniformly and fully mixing the high titanium blast furnace slag, the waste glass powder, a fluxing agent, a foaming agent and a foam stabilizer, pressing into a block, adding the mixture block into a heating device and preparing the microcrystalline foam glass at a low temperature according to a specific heat treatment process by using a one-step sintering method. According to the characteristic that the high titanium blast furnace slag which is rich in TiO2 can serve as a nucleation agent, the low-melting-point waste glass powder serves as a silicious raw material, a proper amount of corresponding fluxing agent and sintering process are matched, the preparation temperature is greatly reduced, and the preparation can be finished through one-step sintering; and therefore, the energy consumption can be reduced, the process is simplified, the cycle is shortened, the cost is saved, the product which is uniform in cells, moderate in cell diameter, low in volume density, low in water absorption rate, good in thermal insulation effect and high in mechanical strength can be obtained, and the additional value of high titanium blast furnace slag utilization is improved.
Owner:SICHUAN UNIV

Ethylene propylene diene terpolymer sponge rubber and preparation method thereof

The invention provides an ethylene propylene diene terpolymer sponge rubber and a preparation method thereof, relating to a rubber and a preparation method thereof. The ethylene propylene diene terpolymer sponge rubber is prepared from ethylene propylene diene terpolymer, a foaming agent, a filling enhancer, a plasticizer, molecular sieve powder with a hygroscopic effect, a vulcanizing agent and a vulcanizing aid. The ethylene propylene diene terpolymer sponge rubber is characterized in that the molecular sieve powder is used for replacing traditional talc powder or calcium carbonate to be used as a filling agent, a foaming agent azobisformamide (AC) and a foaming agent 4,4'-oxy bis(benzenesulfonyl hydrazide) (OBSH) are combined and matched with an accelerant, and the decomposing rate of the foaming agent and the vulcanizing rate of the ethylene propylene diene terpolymer are matched, thus a microporous sponge rubber sealing product with a hygroscopic function is prepared under die pressing vulcanization conditions. The tensile strength, elongation percentage, stress at definite elongation, compression set and other indexes of the ethylene propylene diene terpolymer sponge rubber can meet the use performance requirements of sponge sealing strips; and at the same time, the sponge rubber has uniform foam pores, small density and hygroscopic function.
Owner:JINGDONG RUBBER

Method for preparing polyvinyl alcohol and polyurethane super absorbent sponge

The invention discloses a method for preparing a polyvinyl alcohol and polyurethane super absorbent sponge. The method includes mixing polyvinyl alcohol with distilled water at first, dissolving the polyvinyl alcohol for 20 to 30 minutes under the condition that the water bath temperature ranges from 50 DEG C to 95 DEG C and rotational speed ranges from 400r/min to 600r/min to obtain polyvinyl alcohol aqueous solution; and then heating the polyvinyl alcohol aqueous solution until the temperature of the polyvinyl alcohol aqueous solution ranges from 30 DEG C to 100 DEG C, adding water-based polyurethane prepolymer, catalysts and auxiliary foaming agents into the polyvinyl alcohol aqueous solution, stirring and uniformly mixing the mixture under the condition of rotational speed ranging from 400r/min to 600r/min, enabling the mixture to react for 5 minutes to 10 minutes, and solidifying the mixture for 2 to 4 hours at the temperature ranging from 30 DEG C to 100 DEG C to obtain the sponge with the water absorbent rate higher than 9.8. The water absorbent rate of the obtained sponge is increased to 10-20 times from the original 6-8 times of an existing polyvinyl acetal sponge, the water absorbing velocity of the sponge is increased to 8g/ming from the original 4g/ming, and the polyvinyl alcohol and polyurethane super absorbent sponge has a broad development prospect in fields of aquatic product processing, food, clinical medicine, water treatment and the like.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method of graphene oxide and polyvinyl alcohol hybrid aerogel

The invention belongs to the technical field of preparation of aerogel having a water treatment function, in particular relates to a preparation method of graphene oxide and polyvinyl alcohol hybrid aerogel. The preparation method comprises the following five processing steps: preparing a graphene oxide dispersing solution; preparing a graphene oxide/chitosan mixed solution; preparing a self-foaming solution; preparing a gel solution; preparing graphene oxide/chitosan and polyvinyl alcohol hybrid aerogel. The preparation method is characterized in that the graphene oxide and polyvinyl alcohol hybrid aerogel is prepared by fully mixing the graphene oxide dispersing solution with distilled water, glacial acetic acid and chitosan powder and then adding polyvinyl alcohol, a filling agent, a cross-linking agent, a foaming agent and a catalyst in the mixture. The graphene oxide and polyvinyl alcohol hybrid aerogel prepared by the invention is strong in water absorbing capacity, high in hydrophily and quick in adsorption rate and can be reused after regeneration and can be used for industrial wastewater treatment. The preparation method of the graphene oxide and polyvinyl alcohol hybrid aerogel, disclosed by the invention, has the advantages that the principle is simple, the operation is easy, processing equipment is simple, the cost of raw materials is low, and the preparation method is beneficial for industrialization.
Owner:QINGDAO UNIV

Method and device for directly preparing polylactic acid foam product from polylactic acid polymer melt

ActiveCN109776848AGuaranteed qualityGuaranteed foamabilityApparent densityCrystallinity
The invention provides a method and a device for directly preparing a polylactic acid foam product from a polylactic acid polymerization melt. The method and the device for directly preparing the polylactic acid foam product from the polylactic acid polymerization melt comprises the steps of polylactic acid melt preparation, material feeding and secondary extruding treatment. In the secondary extruding treatment, the outlet pressure of a first-stage double-screw extruder is 15-17 MPa, the material feeding speed of the polylactic acid polymerization melt is 250 kg / h, the foam auxiliary feedingspeed is 7.5-10 kg / h, and the foaming gas feeding speed is 2.8-7.5 L / h. The method and the device for directly preparing the polylactic acid foam product from the polylactic acid polymerization melt,provided by the invention, have the advantages that an influence on the foaming performance is avoided due to no need of processes such as water cooled pelletizing, repeated drying cooling and heating, melting and mixing; the foaming performance can be guaranteed; the quality can also be guaranteed; the energy consumption is saved by about 1 / 3 or above; the foaming multiplying power of an obtainedproduct is adjusted by 3-25 times; the degree of crystallinity is 40.3-48.5%; the tensile strength is 8.7-19.6 MPa; and the apparent density is 0.05-0.4 g / cm<3>.
Owner:CHTC BIO BASED MATERIAL ENG & TECH NINGBO CO LTD

Preparation method for thermoplastic polyurethane elastomer foaming material

The invention discloses a preparation method for a thermoplastic polyurethane elastomer foaming material. The method comprises the following steps: (1) stirring and mixing 100 parts of TPU material, 0.5-10 parts of graphene material and 0.05-3 parts of lubricating agent, thereby acquiring a mixture; (2) adding the aggregates acquired in the step (1) and water into a reaction kettle and starting to stir; (3) introducing carbon dioxide or / and nitrogen into the reaction kettle, controlling the pressure and temperature in the reaction kettle and keeping the carbon dioxide or / and nitrogen in the reaction kettle under a super-critical state; (4) heating the reaction kettle and dissolving the super-critical carbon dioxide or / and nitrogen in thermoplastic polyurethane with uniformly doped graphene under the temperature of the reaction kettle; (5) continuously adding a foaming agent, a cross-linking agent, a lubricating agent and cross-linking auxiliaries into the reaction kettle, continuously stirring for 1-5h, and then connecting the reaction kettle with a pressure tank and enabling the materials in the reaction kettle to enter into the pressure tank under the pressure effect; and (6) foaming the materials in the pressure tank for 30-90min, and then reducing the pressure and reducing the temperature to below 70 DEG C, thereby acquiring the TPU foaming material.
Owner:XIFENG 2D FUJIAN MATERIAL TECH CO LTD

Thermal conductive polyurethane synthetic leather production method

The invention discloses a thermal conductive polyurethane synthetic leather production method which comprises the following process: selecting base cloth, coating with wet process polyurethane slurry, solidifying, washing with water, expanding and drying, veneering by dry method, and finishing the surface; first of all, the base cloth is coated with the wet process polyurethane slurry with conductive filler; then, the coated substrate is solidified by wet method for adjusting of bubble hole structure and expanding and drying for production of thermal conductive and breathable Base; finally thermal conductive breathable polyurethane synthetic leather is produced by veneering by dry method and finishing the surface of the thermal conductive and breathable Base. The thermal conductive polyurethane synthetic leather prepared by the method is relatively high in thermal conductivity coefficient, the thermal conductivity coefficient reaches 0.06-0.09W .M <-1> .K <-1>, compared with traditional synthetic leather, the thermal conductivity is increased by more than 30%, and the bubble hole is even, delicate, soft in hand feeling, good in drapability, air and moisture permeability, similar to natural leather in apparent and hand feeling, and simple in manufacturing process.
Owner:SHAANXI UNIV OF SCI & TECH

Method for preparing rubber-toughened PS foam material through extrusion of supercritical fluid

The invention discloses a method for preparing rubber-toughened PS foam material through extrusion of a supercritical fluid. The rubber-toughened PS foam material is prepared from the following raw materials in parts by weight: 80-95 parts of polystyrene, 5-20 parts of a thermoplastic elastomer and 1-10 parts of one or more nucleating agents. The method comprises the following steps: mixing such raw materials according to a proportion; feeding the mixed raw materials into a first extruder for melt-blending and extrusion pelletization to obtain a rubber-toughened polystyrene-based blend containing the nucleating agents; feeding the rubber-toughened polystyrene-based blend into a second extruder for heating and melting; meanwhile, injecting the supercritical fluid into a plasticization section of the second extruder to ensure that a homogeneous phase system is formed between the supercritical fluid and a melt of the rubber-toughened polystyrene-based blend under the shearing action of a threaded rod of the second extruder; continuously extruding the supercritical fluid for foaming. The rubber-toughened PS foam material prepared according to the method is uniform in cell, small in cell size, high in processing operability and anti-impact property, and suitable for industrialized production.
Owner:SOUTH CHINA UNIV OF TECH

Natural rubber white odorless spongy cushion for in situ color-protecting shoes and preparation method thereof

ActiveCN102391550APrevent high temperature agingShort vulcanization timeInsolesLaminationActivated carbonPolymer science
The invention discloses a natural rubber white odorless spongy cushion for in situ color-protecting shoes and a preparation method thereof. The raw materials of the spongy cushion comprises natural rubber, sulfur, an accelerating agent, a vulcanizing active agent, a hole-forming agent AC (activated carbon), titanium white, 5# engine oil, kaolin, a rubber odor-removing agent and a foaming agent OBSH (oxybis(benzenesulfonyl hydrazide)). In the invention, the odorless spongy for shoes is prepared by utilizing the natural rubber as a main body; vulcanization is promoted by using a thiuram accelerating agent TMTD (tetramethyl thiuram disulfide) to inhibit the high-temperature ageing of the natural rubber, thereby ensuring that titanium white and kaolin filled white spongy rubber do not generate high yellowing to discolor the bottom surfaces in the shoes; the foaming agent AC and OBSH are jointly used, so as to achieve the shape keeping property and even bubbles and low odor of the inner bottoms of the spongy shoes; because no water gas is generated in the foaming process of spongy, heterochromatic substances are not dissolved and transported to cause the yellowing and discoloring of white soft goods of the inner bottoms of the shoes, thus the spongy cushion has abundant white keeping capacity; and the odor generated in the process of vulcanizing the spongy rubber can be effectively removed through the rubber odor-removing agent.
Owner:际华制鞋工业有限公司
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