A kind of asymmetric PVDF coated diaphragm and preparation method thereof
An asymmetric, coating technology, applied in the direction of structural parts, electrical components, battery pack components, etc., can solve the problems of battery electrical performance decline, battery performance decline, failure to take into account, etc., to improve consistency, adhesion, etc. Keep the force consistent and ensure the effect of electrical performance
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Embodiment 1
[0032] (1) Preparation of PVDF slurry:
[0033] A. Preparation of the first PVDF slurry: the first PVDF slurry is obtained by mixing 1% of binder, 86% of deionized water, 8% of PVDF monomer, and 5% of auxiliary agent;
[0034] B. Preparation of the second PVDF slurry: 3% of binder, 86.9% of deionized water, 10% of PVDF monomer, and 0.1% of auxiliary agent are mixed to obtain the second PVDF slurry;
[0035] (2) Coating diaphragm:
[0036] A. Select the substrate, coat the second PVDF slurry on the lower surface of the substrate at a speed of 80m / min to obtain a second PVDF coating, and place the second PVDF coating at 60°C for two dryings, one drying 30s to obtain diaphragm A; the areal density of the second PVDF coating is 0.5g / m 2 ;
[0037] B. Coating the first PVDF slurry on the upper surface of the substrate at a speed of 80 m / min to obtain the first PVDF coating, placing the first PVDF coating at 60°C and drying for 30 s to obtain an asymmetric PVDF coating Separator...
Embodiment 2
[0039] (1) Preparation of PVDF slurry:
[0040] A. Preparation of the first PVDF slurry: 3% of binder, 90% of deionized water, 1% of PVDF monomer, and 6% of auxiliary agent are mixed to obtain the first PVDF slurry;
[0041] B. Preparation of the second PVDF slurry: 3% of binder, 75% of deionized water, 20% of PVDF monomer, and 2% of auxiliary agent are mixed to obtain the second PVDF slurry;
[0042] (2) Coating diaphragm:
[0043] A. Select the substrate, coat the second PVDF slurry on the lower surface of the substrate at a speed of 80m / min to obtain a second PVDF coating, and place the second PVDF coating at 60°C for two dryings, one drying 30s to obtain diaphragm A; the areal density of the second PVDF coating is 0.5g / m 2 ;
[0044] B. Coating the first PVDF slurry on the upper surface of the substrate at a speed of 80 m / min to obtain the first PVDF coating, placing the first PVDF coating at 60°C and drying for 30 s to obtain an asymmetric PVDF coating Separator; firs...
Embodiment 3
[0046] (1) Preparation of PVDF slurry:
[0047]A. Preparation of the first PVDF slurry: the first PVDF slurry is obtained by mixing 5% of binder, 90% of deionized water, 0.1% of PVDF monomer, and 4.9% of auxiliary agent;
[0048] B. Preparation of the second PVDF slurry: 5% of binder, 75% of deionized water, 10% of PVDF monomer, and 10% of auxiliary agent are mixed to obtain the second PVDF slurry;
[0049] (2) Coating diaphragm:
[0050] A. Select the substrate, coat the second PVDF slurry on the lower surface of the substrate at a speed of 80m / min to obtain a second PVDF coating, and place the second PVDF coating at 60°C for two dryings, one drying 30s to obtain diaphragm A; the areal density of the second PVDF coating is 0.5g / m 2 ;
[0051] B. Coating the first PVDF slurry on the upper surface of the substrate at a speed of 80 m / min to obtain the first PVDF coating, placing the first PVDF coating at 60°C and drying for 30 s to obtain an asymmetric PVDF coating Separator...
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