A kind of high-capacity silicon-carbon material for negative electrode of lithium battery and preparation method thereof
A silicon-carbon material, high-capacity technology, applied in the field of electrochemistry, can solve the problems of increasing production cost, weak binding force, reducing efficiency and product yield, etc., to achieve the effect of improving conductivity, reducing possibility, and improving stability
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Embodiment 1
[0045] In this embodiment, the preparation method of the highly stable silicon-carbon negative electrode material for lithium batteries is as follows:
[0046] (1) Disperse 2g of nano-silicon in 100mL of ethanol, ultrasonically disperse and stir evenly, and add 10g of chitosan aqueous solution with a concentration of 10% drop by drop to obtain dispersion A;
[0047] (2) Disperse 0.05g of carbon nanofibers in 100mL of ethanol to obtain dispersion B;
[0048] (3) Disperse 4g of graphite intermediate in 100mL of ethanol, ultrasonically and stir evenly, and dropwise add 0.5g of amino polyether silicone with a concentration of 50% to obtain dispersion D;
[0049] (4) Add dispersion A, 0.5g of WD-50 with a concentration of 100%, and dispersion B to dispersion D dropwise at the same time, control the rotation speed at 500rad / min, and stir at 80°C for 12 hours to obtain dispersion E ;
[0050] (5) Let the dispersion E stand still for 2 hours, collect the lower layer slurry, filter i...
Embodiment 2
[0053] In this embodiment, the preparation method of the highly stable silicon-carbon negative electrode material for lithium batteries is as follows:
[0054] (1) Disperse 5g of nano-silicon in 100mL of ethanol, ultrasonically disperse and stir evenly, and add 2g of 50% phytic acid aqueous solution drop by drop to obtain dispersion A;
[0055] (2) Disperse 0.1g of carbon nanotubes in 100mL of ethanol to obtain dispersion B;
[0056] (3) Disperse 5g of graphite intermediate in 100mL of ethanol, ultrasonically and stir evenly, and dropwise add 0.5g of WD-50 with a concentration of 100% to obtain dispersion D;
[0057] (4) Add dispersion A, 0.5g of WD-50 with a concentration of 100%, and dispersion B to dispersion D dropwise at the same time, control the speed at 1000rad / min, and stir at 60°C for 4 hours to obtain dispersion E ;
[0058] (5) Let the dispersion E stand still for 4 hours, pour off the supernatant to obtain the lower layer slurry, centrifuge it, dry it in vacuum ...
Embodiment 3
[0061] In this embodiment, the preparation method of the highly stable silicon-carbon negative electrode material for lithium batteries is as follows:
[0062] (1) Disperse 4g of nano-silicon in 100mL of isopropanol, ultrasonically disperse and stir evenly, and add 1.5g of 30% sucrose solution drop by drop to obtain dispersion A;
[0063] (2) Disperse 0.02g of carbon nanotubes in 100mL of isopropanol to obtain dispersion B;
[0064] (3) Disperse 2g of mesocarbon microsphere intermediate in 100mL of isopropanol, ultrasonically and stir evenly, and dropwise add 0.4g of KH550 with a concentration of 50% to obtain dispersion D;
[0065] (4) Add dispersion A, 0.4 g of KH550 with a concentration of 50%, and dispersion B to dispersion D dropwise at the same time, control the speed at 1500 rad / min, and stir at 40°C for 8 hours to obtain dispersion E;
[0066] (5) Let the dispersion E stand still for 3 hours, collect the slurry in the lower layer, dry it in a blast oven at 70°C for 4 ...
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