Polyamide fiber containing olive and preparation method of polyamide fiber

A nylon fiber and olive technology is applied in the field of olive-containing nylon fiber and its preparation, which can solve the problems of poor distribution, inconsistent nylon fiber performance, unsatisfactory modification effect, etc. Ineffective, tight and firm effect

Inactive Publication Date: 2021-01-22
BESTEE MATERIAL (TSINGTAO) CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The applicant found through research that in the process of preparing nylon fibers by the above-mentioned process, due to the characteristic that nano-silica particles tend to agglomerate, when used as a carrier loaded with functional components, their distribution inside the fiber is not good. The modification effect is unsatisfactory, and the characteristics of the functional components cannot fully exert the modification effect on the fiber
[0009] Furthermore, the applicant found in the process of using olive as a plant modification material to modify nylon that when the active ingredients extracted from olives were loaded on a common carrier, the loading effect was not ideal and the process requirements could not be met.
And when the described active ingredient is loaded on the nano-silica particles, although the loading effect is better, its processing stability is not ideal, and the properties of different batches of nylon fiber products are inconsistent, which affects the large-scale production of functional nylon fiber products. , standardized production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] A method for preparing olive-containing nylon fibers, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.

[0046] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts are mixed, ground to 150 mesh; put into 10 times the volume of absolute ethanol, stirred at 100RPM for 10min, heated to 40°C, and Ultrasonic extraction was performed for 1 h, and the solid matter was filtered out to obtain the olive extract.

[0047] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.

[0048] The weight ratio of the olive leaf extract: olive fruit extract is 1:5.

[0049] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.

[00...

Embodiment 2

[0078] A method for preparing olive-containing nylon fibers, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.

[0079] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts were mixed, ground to 200 mesh; put into 10 times the volume of absolute ethanol, stirred at 150RPM for 15min, heated to 50°C, and carried out Ultrasonic extraction for 1.5 h, and the solid matter was filtered out to obtain the olive extract.

[0080] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.

[0081] The weight ratio of the olive leaf extract: olive fruit extract is 1:6.

[0082] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.

[0...

Embodiment 3

[0111] A method for preparing olive-containing nylon fiber, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.

[0112] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts were mixed, ground to 200 mesh; put into 10 times the volume of absolute ethanol, stirred at 150RPM for 15min, heated to 50°C, and carried out Ultrasonic extraction for 1.5 h, and the solid matter was filtered out to obtain the olive extract.

[0113] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.

[0114] The weight ratio of the olive leaf extract: olive fruit extract is 1:6.

[0115] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.

[01...

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Abstract

The invention provides polyamide fiber containing olive and a preparation method of the polyamide fiber. The preparation method comprises the following steps: preparation of an olive extracting solution, preparation of porous nanoparticles, preparation of porous nanoparticles containing an olive extract and preparation of functional master batch. The preparation method disclosed by the invention has the beneficial effects that the prepared porous nanoparticles containing the olive extract are good in distribution in the fiber, the antibacterial rate of the polyamide fiber to staphylococcus aureus is greater than or equal to 99.8%, the antibacterial rate of the polyamide fiber to escherichia coli is greater than or equal to 95.4%, and the antibacterial rate of the polyamide fiber to candidaalbicans is greater than or equal to 92.7%; the breaking strength of the polyamide fiber is greater than or equal to 6.2 cN / dtex, the elongation at break of the polyamide fiber is greater than or equal to 39%, and the yellowing resistance class of the polyamide fiber is 5.

Description

technical field [0001] The invention relates to the field of nylon fibers, in particular to olive-containing nylon fibers and a preparation method thereof. Background technique [0002] Olive, arbor plant of the family Olivaceae. It can reach a height of 35 meters and a diameter at breast height of 150 centimeters. 3-6 pairs of leaflets, papery to leathery, 12-16 pairs of lateral veins, infructescence 1.5-15 cm long, with 1-6 fruits. Oval to spindle-shaped, yellow-green when mature, thick exocarp, hard core, pointed at both ends, and roughened nuclear surface. The flowering period is from April to May, and the fruit matures from October to December. Olives are native to southern China and are cultivated in Fujian, China, Taiwan, Guangdong, Guangxi, Yunnan, Japan (Nagasaki, Okinawa) and the Malay Peninsula. Wild olives are found in valleys and hillside miscellaneous forests below 1,300 meters above sea level. , or cultivated in gardens and villages. [0003] Olive is a g...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/90D01F1/10
CPCD01F1/10D01F1/103D01F6/90
Inventor 黄效华甄丽刘潇黄效龙穆伟华
Owner BESTEE MATERIAL (TSINGTAO) CO LTD
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